2,3,5,6-tetramethyl-5-(2,3,4-trimethoxyphenyl)-4-oxocyclohexa-1,2-dienyl 2-chloroacetate

Base Information

Chemical Name:2,3,5,6-tetramethyl-5-(2,3,4-trimethoxyphenyl)-4-oxocyclohexa-1,2-dienyl 2-chloroacetate
CAS No.:335642-41-6
Molecular Formula:C₂₁H₂₅ClO₆
Molecular Weight:408.879
Hs Code.:

Synonyms:2,3,5,6-tetramethyl-5-(2,3,4-trimethoxyphenyl)-4-oxocyclohexa-1,2-dienyl 2-chloroacetate

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Chemical Property of 2,3,5,6-tetramethyl-5-(2,3,4-trimethoxyphenyl)-4-oxocyclohexa-1,2-dienyl 2-chloroacetate

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Technology Process of 2,3,5,6-tetramethyl-5-(2,3,4-trimethoxyphenyl)-4-oxocyclohexa-1,2-dienyl 2-chloroacetate

There total 12 articles about 2,3,5,6-tetramethyl-5-(2,3,4-trimethoxyphenyl)-4-oxocyclohexa-1,2-dienyl 2-chloroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 634-36-6
1,2,3-trimethoxybenzene

: chloro-acetic acid 2,3,5,6-tetramethyl-4-oxo-1-(2,4,6-trifluoro-phenylsulfanyl)-cyclohexa-2,5-dienyl ester

: C₁₅H₁₃F₃O₃S

: 335642-41-6
2,3,5,6-tetramethyl-5-(2,3,4-trimethoxyphenyl)-4-oxocyclohexa-1,2-dienyl 2-chloroacetate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 0 ℃; for 0.166667h; Further Variations:; Reaction partners; Temperatures; Product distribution;
DOI:10.1016/S0040-4039(00)02186-9

Reference yield: 76.0%

: 634-36-6
1,2,3-trimethoxybenzene

: 335642-24-5
2,3,5,6-tetramethyl-1-(4-nitrophenylthio)-4-oxocyclohexa-2,5-dienyl 2-chloroacetate

: 1,2,3-trimethoxy-4-(4-nitrophenylthio)benzene

: 335642-41-6
2,3,5,6-tetramethyl-5-(2,3,4-trimethoxyphenyl)-4-oxocyclohexa-1,2-dienyl 2-chloroacetate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 0 ℃; for 0.166667h;
DOI:10.1016/S0040-4039(00)02186-9 DOI:10.1021/jo001710q

Reference yield: 46.0%

: 634-36-6
1,2,3-trimethoxybenzene

: 335642-18-7
1-(4-chlorophenylthio)-2,3,5,6-tetramethyl-4-oxocyclohexa-2,5-dienyl 2-chloroacetate

: 335642-41-6
2,3,5,6-tetramethyl-5-(2,3,4-trimethoxyphenyl)-4-oxocyclohexa-1,2-dienyl 2-chloroacetate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 0 ℃; for 0.166667h;
DOI:10.1016/S0040-4039(00)02186-9