1-(4-fluorophenylthio)-2,3,5,6-tetramethyl-4-oxocyclohexa-2,5-dienyl 2-chloroacetate

Base Information

Chemical Name:1-(4-fluorophenylthio)-2,3,5,6-tetramethyl-4-oxocyclohexa-2,5-dienyl 2-chloroacetate
CAS No.:335642-20-1
Molecular Formula:C₁₈H₁₈ClFO₃S
Molecular Weight:368.857
Hs Code.:

Synonyms:1-(4-fluorophenylthio)-2,3,5,6-tetramethyl-4-oxocyclohexa-2,5-dienyl 2-chloroacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-fluorophenylthio)-2,3,5,6-tetramethyl-4-oxocyclohexa-2,5-dienyl 2-chloroacetate

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Technology Process of 1-(4-fluorophenylthio)-2,3,5,6-tetramethyl-4-oxocyclohexa-2,5-dienyl 2-chloroacetate

There total 2 articles about 1-(4-fluorophenylthio)-2,3,5,6-tetramethyl-4-oxocyclohexa-2,5-dienyl 2-chloroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 89728-00-7
1-ethoxyvinyl 2-chloroacetate

: 169216-75-5
4-(4-Fluoro-benzenesulfinyl)-2,3,5,6-tetramethyl-phenol

: 335642-20-1
1-(4-fluorophenylthio)-2,3,5,6-tetramethyl-4-oxocyclohexa-2,5-dienyl 2-chloroacetate

Guidance literature:: With toluene-4-sulfonic acid; In toluene; at 60 ℃; for 1h;
DOI:10.1021/jo001710q

Reference yield:

: 541-88-8
Chloroacetic anhydride

: 169216-75-5
4-(4-Fluoro-benzenesulfinyl)-2,3,5,6-tetramethyl-phenol

: 335642-20-1
1-(4-fluorophenylthio)-2,3,5,6-tetramethyl-4-oxocyclohexa-2,5-dienyl 2-chloroacetate

Guidance literature:: DOI:10.1016/S0040-4039(00)02186-9

Reference yield: 25.0%

: 634-36-6
1,2,3-trimethoxybenzene

: 335642-20-1
1-(4-fluorophenylthio)-2,3,5,6-tetramethyl-4-oxocyclohexa-2,5-dienyl 2-chloroacetate

: 4-(4-fluorophenylthio)-1,2,3-trimethoxybenzene

: 335642-41-6
2,3,5,6-tetramethyl-5-(2,3,4-trimethoxyphenyl)-4-oxocyclohexa-1,2-dienyl 2-chloroacetate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 0 ℃; for 0.166667h;
DOI:10.1016/S0040-4039(00)02186-9