methyl 2-diazo-3-oxo-6-phenyl-4-propylhexanoate

Base Information

Chemical Name:methyl 2-diazo-3-oxo-6-phenyl-4-propylhexanoate
CAS No.:104620-16-8
Molecular Formula:C₁₆H₂₀N₂O₃
Molecular Weight:288.346
Hs Code.:

Synonyms:methyl 2-diazo-3-oxo-6-phenyl-4-propylhexanoate

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Chemical Property of methyl 2-diazo-3-oxo-6-phenyl-4-propylhexanoate

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Technology Process of methyl 2-diazo-3-oxo-6-phenyl-4-propylhexanoate

There total 4 articles about methyl 2-diazo-3-oxo-6-phenyl-4-propylhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 104620-15-7
methyl 3-oxo-6-phenyl-4-propylhexanoate

: 104620-16-8
methyl 2-diazo-3-oxo-6-phenyl-4-propylhexanoate

Guidance literature:: With triethylamine; Methanesulfonyl azide; In acetonitrile; for 3h; Ambient temperature;
DOI:10.1021/ja00284a037

Reference yield:

: 591-78-6
n-hexan-2-one

: 104620-16-8
methyl 2-diazo-3-oxo-6-phenyl-4-propylhexanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 48 percent / 50 percent NaH oil disp. / tetrahydrofuran / 12 h / Ambient temperature

2: 19 percent / n-BuLi, diisopropylamine / tetrahydrofuran / -78 °C

3: 98 percent / methanesulfonyl azide, triethylamine / acetonitrile / 3 h / Ambient temperature

With n-butyllithium; sodium hydride; triethylamine; diisopropylamine; Methanesulfonyl azide; In tetrahydrofuran; acetonitrile;
DOI:10.1021/ja00284a037

Reference yield:

: 39815-78-6
methyl 3-oxoheptanoate

: 104620-16-8
methyl 2-diazo-3-oxo-6-phenyl-4-propylhexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 19 percent / n-BuLi, diisopropylamine / tetrahydrofuran / -78 °C

2: 98 percent / methanesulfonyl azide, triethylamine / acetonitrile / 3 h / Ambient temperature

With n-butyllithium; triethylamine; diisopropylamine; Methanesulfonyl azide; In tetrahydrofuran; acetonitrile;
DOI:10.1021/ja00284a037