methyl 3-oxo-6-phenyl-4-propylhexanoate

Base Information Edit

Chemical Name:methyl 3-oxo-6-phenyl-4-propylhexanoate
CAS No.:104620-15-7
Molecular Formula:C₁₆H₂₂O₃
Molecular Weight:262.349
Hs Code.:
Mol file:104620-15-7.mol

Synonyms:methyl 3-oxo-6-phenyl-4-propylhexanoate

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Chemical Property of methyl 3-oxo-6-phenyl-4-propylhexanoate Edit

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Technology Process of methyl 3-oxo-6-phenyl-4-propylhexanoate

There total 2 articles about methyl 3-oxo-6-phenyl-4-propylhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 39815-78-6
methyl 3-oxoheptanoate

: 103-63-9
1-phenyl-2-bromoethane

: 104620-15-7
methyl 3-oxo-6-phenyl-4-propylhexanoate

Guidance literature:: With n-butyllithium; diisopropylamine; In tetrahydrofuran; at -78 ℃;
DOI:10.1021/ja00284a037

Reference yield:

: 591-78-6
n-hexan-2-one

: 104620-15-7
methyl 3-oxo-6-phenyl-4-propylhexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 48 percent / 50 percent NaH oil disp. / tetrahydrofuran / 12 h / Ambient temperature

2: 19 percent / n-BuLi, diisopropylamine / tetrahydrofuran / -78 °C

With n-butyllithium; sodium hydride; diisopropylamine; In tetrahydrofuran;
DOI:10.1021/ja00284a037