(S)-N-(1-(2,2-dimethyl-1,3-dioxolan-4-yl)ethylidene)-1-phenylmethanamine

Base Information

Chemical Name:(S)-N-(1-(2,2-dimethyl-1,3-dioxolan-4-yl)ethylidene)-1-phenylmethanamine
CAS No.:180839-79-6
Molecular Formula:C₁₄H₁₉NO₂
Molecular Weight:233.31
Hs Code.:

Synonyms:(S)-N-(1-(2,2-dimethyl-1,3-dioxolan-4-yl)ethylidene)-1-phenylmethanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N-(1-(2,2-dimethyl-1,3-dioxolan-4-yl)ethylidene)-1-phenylmethanamine

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Technology Process of (S)-N-(1-(2,2-dimethyl-1,3-dioxolan-4-yl)ethylidene)-1-phenylmethanamine

There total 1 articles about (S)-N-(1-(2,2-dimethyl-1,3-dioxolan-4-yl)ethylidene)-1-phenylmethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61821-86-1
(R)-2,2-dimethyl-1,3-dioxolan-4-yl methyl ketone

: 100-46-9
benzylamine

: 180839-79-6
(S)-N-(1-(2,2-dimethyl-1,3-dioxolan-4-yl)ethylidene)-1-phenylmethanamine

Guidance literature:: With titanium tetrachloride; triethylamine; In dichloromethane; at -78 ℃; for 1.5h;
DOI:10.1021/jo962017z

Reference yield: 65.0%

: 19810-31-2
Benzyloxyacetyl chloride

: 180839-79-6
(S)-N-(1-(2,2-dimethyl-1,3-dioxolan-4-yl)ethylidene)-1-phenylmethanamine

: 180839-80-9
(3R,4S)-1-Benzyl-3-benzyloxy-4-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-methyl-azetidin-2-one

Guidance literature:: With triethylamine; In dichloromethane; at -78 - 20 ℃; for 20h;
DOI:10.1021/jo962017z

Reference yield: 64.0%

: 180839-79-6
(S)-N-(1-(2,2-dimethyl-1,3-dioxolan-4-yl)ethylidene)-1-phenylmethanamine

: 192764-17-3
(S)-N-benzyl-1-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]ethanamine

: 192764-16-2
(R)-N-benzyl-1-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]ethanamine

Guidance literature:: (S)-N-(1-(2,2-dimethyl-1,3-dioxolan-4-yl)ethylidene)-1-phenylmethanamine; With sodium tetrahydroborate; In ethanol; at -78 ℃; for 1.5h; Inert atmosphere;

With water; ammonium chloride; optical yield given as %de; diastereoselective reaction;
DOI:10.1016/j.tetasy.2010.02.012