2-butyl-4-phenyl-2-<(2,4,6-tri-tert-butylphenyl)amino>-3-(2,4,6-tri-tert-butylphenyl)-1-oxa-3-aza-2-silacyclobutane

Base Information

Chemical Name:2-butyl-4-phenyl-2-<(2,4,6-tri-tert-butylphenyl)amino>-3-(2,4,6-tri-tert-butylphenyl)-1-oxa-3-aza-2-silacyclobutane
CAS No.:136630-53-0
Molecular Formula:C₄₇H₇₄N₂OSi
Molecular Weight:711.203
Hs Code.:

Synonyms:2-butyl-4-phenyl-2-<(2,4,6-tri-tert-butylphenyl)amino>-3-(2,4,6-tri-tert-butylphenyl)-1-oxa-3-aza-2-silacyclobutane

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Chemical Property of 2-butyl-4-phenyl-2-<(2,4,6-tri-tert-butylphenyl)amino>-3-(2,4,6-tri-tert-butylphenyl)-1-oxa-3-aza-2-silacyclobutane

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Technology Process of 2-butyl-4-phenyl-2-<(2,4,6-tri-tert-butylphenyl)amino>-3-(2,4,6-tri-tert-butylphenyl)-1-oxa-3-aza-2-silacyclobutane

There total 4 articles about 2-butyl-4-phenyl-2-<(2,4,6-tri-tert-butylphenyl)amino>-3-(2,4,6-tri-tert-butylphenyl)-1-oxa-3-aza-2-silacyclobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 100-52-7
benzaldehyde

: 136630-58-5
lithium N,N'-bis(2,4,6-tri-tert-butylphenyl)-n-butyl-silylaamidide

: 136630-53-0
2-butyl-4-phenyl-2-<(2,4,6-tri-tert-butylphenyl)amino>-3-(2,4,6-tri-tert-butylphenyl)-1-oxa-3-aza-2-silacyclobutane

Guidance literature:: In diethyl ether; for 1h;
DOI:10.1021/ja00022a035

Reference yield:

: 4074-25-3
2,4,6-tri-tert-butylnitrobenzene

: 136630-53-0
2-butyl-4-phenyl-2-<(2,4,6-tri-tert-butylphenyl)amino>-3-(2,4,6-tri-tert-butylphenyl)-1-oxa-3-aza-2-silacyclobutane

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / Na/Hg, MeOH / 12 h / Heating

2: 1.) n-BuLi, 2.) SiCl₄ / 1.) hexane, reflux, 2 h, 2.) hexane, reflux, 48 h

3: 73 percent / diethyl ether; hexane / 1.) -78 deg C, 3 h, 2.) RT, 24 h

4: 44 percent / diethyl ether / 1 h

With methanol; sodium amalgam; n-butyllithium; tetrachlorosilane; In diethyl ether; hexane;
DOI:10.1021/ja00022a035

Reference yield:

: 961-38-6
2,4,6-Tri-tert-butylaniline

: 136630-53-0
2-butyl-4-phenyl-2-<(2,4,6-tri-tert-butylphenyl)amino>-3-(2,4,6-tri-tert-butylphenyl)-1-oxa-3-aza-2-silacyclobutane

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi, 2.) SiCl₄ / 1.) hexane, reflux, 2 h, 2.) hexane, reflux, 48 h

2: 73 percent / diethyl ether; hexane / 1.) -78 deg C, 3 h, 2.) RT, 24 h

3: 44 percent / diethyl ether / 1 h

With n-butyllithium; tetrachlorosilane; In diethyl ether; hexane;
DOI:10.1021/ja00022a035