(SP,1'R,2'S,5'R)-<2-<(2'-isopropyl-5'-methylcyclohexyl)oxy>ethyl>(o-methoxyphenyl)phenylphosphine oxide

Base Information

Chemical Name:(SP,1'R,2'S,5'R)-<2-<(2'-isopropyl-5'-methylcyclohexyl)oxy>ethyl>(o-methoxyphenyl)phenylphosphine oxide
CAS No.:108035-56-9
Molecular Formula:C₂₅H₃₅O₃P
Molecular Weight:414.525
Hs Code.:

Synonyms:(SP,1'R,2'S,5'R)-<2-<(2'-isopropyl-5'-methylcyclohexyl)oxy>ethyl>(o-methoxyphenyl)phenylphosphine oxide

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Chemical Property of (SP,1'R,2'S,5'R)-<2-<(2'-isopropyl-5'-methylcyclohexyl)oxy>ethyl>(o-methoxyphenyl)phenylphosphine oxide

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Technology Process of (SP,1'R,2'S,5'R)-<2-<(2'-isopropyl-5'-methylcyclohexyl)oxy>ethyl>(o-methoxyphenyl)phenylphosphine oxide

There total 4 articles about (SP,1'R,2'S,5'R)-<2-<(2'-isopropyl-5'-methylcyclohexyl)oxy>ethyl>(o-methoxyphenyl)phenylphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 2216-51-5
(-)-menthol

: 108058-67-9
(-)-(S_P)-(2-methoxyphenyl)phenylvinylphosphine oxide

: 108035-56-9
(SP,1'R,2'S,5'R)-<2-<(2'-isopropyl-5'-methylcyclohexyl)oxy>ethyl>(o-methoxyphenyl)phenylphosphine oxide

Guidance literature:: With sodium hydride; at 60 ℃; for 14h;
DOI:10.1021/jo00387a010

Reference yield:

: 20663-35-8
(S_p)-(2-methoxyphenyl)methylphenylphosphine oxide

: 108035-56-9
(SP,1'R,2'S,5'R)-<2-<(2'-isopropyl-5'-methylcyclohexyl)oxy>ethyl>(o-methoxyphenyl)phenylphosphine oxide

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / LDA, CuCl₂ / tetrahydrofuran; hexane / 1.) -78 deg C, 1 h, 2.) RT, 0.5 h

2: 82 percent / xylene / 1 h / Heating

3: 81 percent / NaH / 14 h / 60 °C

With sodium hydride; copper dichloride; lithium diisopropyl amide; In tetrahydrofuran; hexane; xylene;
DOI:10.1021/jo00387a010

Reference yield:

: 108058-66-8,108058-69-1
(PS,SRS)-S-<2-<(0-methoxyphenyl)phenylphosphinyl>ethyl>-N-methyl-S-phenylsulfoximine

: 108035-56-9
(SP,1'R,2'S,5'R)-<2-<(2'-isopropyl-5'-methylcyclohexyl)oxy>ethyl>(o-methoxyphenyl)phenylphosphine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / xylene / 1 h / Heating

2: 81 percent / NaH / 14 h / 60 °C

With sodium hydride; In xylene;
DOI:10.1021/jo00387a010