Technology Process of C33H42O10
There total 3 articles about C33H42O10 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 93 percent / tetrapropylammonium perruthenate, 4-methylmorpholine N-oxide / acetonitrile / 2 h / 25 °C
2: 1.) BH3*THF, 2.) NaHCO3, H2O2 / 1.) THF, 0 deg C, 3 h, 2.) THF, 25 deg C, 1 h
With
tetrapropylammonium perruthennate; borane-THF; dihydrogen peroxide; sodium hydrogencarbonate; 4-methylmorpholine N-oxide;
In
acetonitrile;
DOI:10.1021/ja00107a009
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 95 percent / 4-(dimethylamino)pyridine / CH2Cl2 / 2 h / 25 °C
2: 93 percent / tetrapropylammonium perruthenate, 4-methylmorpholine N-oxide / acetonitrile / 2 h / 25 °C
3: 1.) BH3*THF, 2.) NaHCO3, H2O2 / 1.) THF, 0 deg C, 3 h, 2.) THF, 25 deg C, 1 h
With
dmap; tetrapropylammonium perruthennate; borane-THF; dihydrogen peroxide; sodium hydrogencarbonate; 4-methylmorpholine N-oxide;
In
dichloromethane; acetonitrile;
DOI:10.1021/ja00107a009
- Guidance literature:
-
With
borane-THF; dihydrogen peroxide; sodium hydrogencarbonate;
Yield given. Multistep reaction. Yields of byproduct given;
1.) THF, 0 deg C, 3 h, 2.) THF, 25 deg C, 1 h;
DOI:10.1021/ja00107a009