C₂₄H₃₂O₇

Base Information

• Chemical Name: C₂₄H₃₂O₇
• CAS No.: 1418031-61-4
• Molecular Formula: C₂₄H₃₂O₇
• Molecular Weight: 432.514
• Mol file: 1418031-61-4.mol

Synonyms:C₂₄H₃₂O₇

Chemical Property of C₂₄H₃₂O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₃₂O₇

There total 8 articles about C₂₄H₃₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

C24H34O7 (1418031-60-3) → C24H32O7 (1418031-61-4)

Guidance literature:

With sodium acetate; pyridinium chlorochromate; In tetrahydrofuran; Inert atmosphere;

DOI:10.1002/anie.201203680

Reference yield:

C30H48O7Si (1418031-59-0) → C24H32O7 (1418031-61-4)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

2: pyridinium chlorochromate; sodium acetate / tetrahydrofuran / Inert atmosphere

With tetrabutyl ammonium fluoride; sodium acetate; pyridinium chlorochromate; In tetrahydrofuran;

DOI:10.1002/anie.201203680

Reference yield:

3-O-benzyl-5-O-[tert-butyl(dimethyl)silyl]-4-(hydroxymethyl)-1,2-O-(1-methylethylidene)-β-L-arabinofuranose (1027758-99-1) → C24H32O7 (1418031-61-4)

Guidance literature:

Multi-step reaction with 5 steps

1: pyridinium chlorochromate; sodium acetate / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere; Microwave irradiation

2: boron trifluoride diethyl etherate / dichloromethane / 3 h / -78 °C / Inert atmosphere

3: pyridine / 24 h / 100 °C / Inert atmosphere

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

5: pyridinium chlorochromate; sodium acetate / tetrahydrofuran / Inert atmosphere

With pyridine; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; sodium acetate; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;

DOI:10.1002/anie.201203680

upstream raw materials:

C₂₅H₄₀O₆Si

C₃₀H₄₈O₇Si

C₂₂H₃₄O₆Si

3-O-benzyl-5-O-[tert-butyl(dimethyl)silyl]-4-(hydroxymethyl)-1,2-O-(1-methylethylidene)-β-L-arabinofuranose