2-Ethyl-benzoic acid [1-amino-1-(3-methoxy-phenyl)-meth-(Z)-ylidene]-hydrazide

Base Information

Chemical Name:2-Ethyl-benzoic acid [1-amino-1-(3-methoxy-phenyl)-meth-(Z)-ylidene]-hydrazide
CAS No.:85681-42-1
Molecular Formula:C₁₇H₁₉N₃O₂
Molecular Weight:297.357
Hs Code.:

Synonyms:2-Ethyl-benzoic acid [1-amino-1-(3-methoxy-phenyl)-meth-(Z)-ylidene]-hydrazide

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Chemical Property of 2-Ethyl-benzoic acid [1-amino-1-(3-methoxy-phenyl)-meth-(Z)-ylidene]-hydrazide

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Technology Process of 2-Ethyl-benzoic acid [1-amino-1-(3-methoxy-phenyl)-meth-(Z)-ylidene]-hydrazide

There total 4 articles about 2-Ethyl-benzoic acid [1-amino-1-(3-methoxy-phenyl)-meth-(Z)-ylidene]-hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.2%

: 55308-52-6
ethyl 3-methoxybenzimidate

: 59635-98-2
2-ethylbenzoic acid hydrazide

: 85681-42-1
2-Ethyl-benzoic acid [1-amino-1-(3-methoxy-phenyl)-meth-(Z)-ylidene]-hydrazide

Guidance literature:: In dichloromethane; for 5h; Heating;
DOI:10.1021/jm00362a018

Reference yield:

: 76118-05-3
2-ethylbenzoyl chloride

: 85681-42-1
2-Ethyl-benzoic acid [1-amino-1-(3-methoxy-phenyl)-meth-(Z)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂ / 2 h

2: 37percent aq. HCl / 0.5 h

3: 87.2 percent / CH₂Cl₂ / 5 h / Heating

With hydrogenchloride; triethylamine; In dichloromethane;
DOI:10.1021/jm00362a018

Reference yield:

: 612-19-1
2-ethylbenzoic acid

: 85681-42-1
2-Ethyl-benzoic acid [1-amino-1-(3-methoxy-phenyl)-meth-(Z)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂ / 2 h / Heating

2: Et₃N / CH₂Cl₂ / 2 h

3: 37percent aq. HCl / 0.5 h

4: 87.2 percent / CH₂Cl₂ / 5 h / Heating

With hydrogenchloride; thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1021/jm00362a018