3-<<(1,1-dimethylethoxy)carbonyl>amino>-12-oxo-2,4,11,14-tetraazapentadec-2-enedioic acid, 1-(1,1-dimethylethyl)ester 15-phenylmethyl ester

Base Information

Chemical Name:3-<<(1,1-dimethylethoxy)carbonyl>amino>-12-oxo-2,4,11,14-tetraazapentadec-2-enedioic acid, 1-(1,1-dimethylethyl)ester 15-phenylmethyl ester
CAS No.:160677-77-0
Molecular Formula:C₂₇H₄₃N₅O₇
Molecular Weight:549.668
Hs Code.:

Synonyms:3-<<(1,1-dimethylethoxy)carbonyl>amino>-12-oxo-2,4,11,14-tetraazapentadec-2-enedioic acid, 1-(1,1-dimethylethyl)ester 15-phenylmethyl ester

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Chemical Property of 3-<<(1,1-dimethylethoxy)carbonyl>amino>-12-oxo-2,4,11,14-tetraazapentadec-2-enedioic acid, 1-(1,1-dimethylethyl)ester 15-phenylmethyl ester

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Technology Process of 3-<<(1,1-dimethylethoxy)carbonyl>amino>-12-oxo-2,4,11,14-tetraazapentadec-2-enedioic acid, 1-(1,1-dimethylethyl)ester 15-phenylmethyl ester

There total 6 articles about 3-<<(1,1-dimethylethoxy)carbonyl>amino>-12-oxo-2,4,11,14-tetraazapentadec-2-enedioic acid, 1-(1,1-dimethylethyl)ester 15-phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 160677-41-8
2-(6-aminohexyl)-1,3-diBocguanidine

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 543-27-1
isobutyl chloroformate

: 160677-77-0
3-<<(1,1-dimethylethoxy)carbonyl>amino>-12-oxo-2,4,11,14-tetraazapentadec-2-enedioic acid, 1-(1,1-dimethylethyl)ester 15-phenylmethyl ester

Guidance literature:: With 4-methyl-morpholine; In tetrahydrofuran; methyl cyclohexane; ethyl acetate;

Reference yield:

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 160677-77-0
3-<<(1,1-dimethylethoxy)carbonyl>amino>-12-oxo-2,4,11,14-tetraazapentadec-2-enedioic acid, 1-(1,1-dimethylethyl)ester 15-phenylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: N-methylmorpholine / tetrahydrofuran / 0.5 h

2: tetrahydrofuran / 26 h / -30 - 20 °C

With 4-methyl-morpholine; In tetrahydrofuran;
DOI:10.1021/jm980431g