methyl 6-O-(4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

Base Information

Chemical Name:methyl 6-O-(4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside
CAS No.:1320337-27-6
Molecular Formula:C₃₈H₃₈O₁₄
Molecular Weight:718.711
Hs Code.:

Synonyms:methyl 6-O-(4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 6-O-(4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

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Technology Process of methyl 6-O-(4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

There total 6 articles about methyl 6-O-(4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 34234-44-1
methyl 2,3,4-tri-O-benzoylglucopyranoside

: ethyl 4,6-di-O-acetyl-2,3-dideoxy-D-erythro-1-thio-hex-2-enopyranoside

: 1320337-27-6
methyl 6-O-(4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at 0 ℃; for 0.25h; Molecular sieve;
DOI:10.1016/j.carres.2011.04.039

Reference yield:

: 34234-44-1
methyl 2,3,4-tri-O-benzoylglucopyranoside

: 2873-29-2
D-glucal triacetate

: 1320337-27-6
methyl 6-O-(4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

: 1629041-76-4
methyl-6-O-(4,6-di-O-acetyl-2,3-dideoxy-β-D-erythro-hex-2-enopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

Guidance literature:: With copper(II) bis(trifluoromethanesulfonate); In acetonitrile; at 20 ℃; for 12h; Overall yield = 62 %; stereoselective reaction; Inert atmosphere; Sealed tube; Green chemistry;
DOI:10.1055/s-0033-1341232

Reference yield:

: 34234-44-1
methyl 2,3,4-tri-O-benzoylglucopyranoside

: 2873-29-2
D-glucal triacetate

: 1320337-27-6
methyl 6-O-(4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

: methyl 6-O-(4,6-di-O-acetyl-2,3-dideoxy-β-D-erythro-hex-2-enopyranosyl)-2,3,4-tris-O-(phenylmethyl)-α-D-glucopyranoside

Guidance literature:: With Fe(III) immobilized on Fe₃O₄ nanoparticles-coated carbon shell; In 1,2-dichloro-ethane; at 25 ℃; for 0.166667h; Overall yield = 86percent; Green chemistry;
DOI:10.1055/s-0037-1611855