cholecalciferol benzoate

Base Information

• Chemical Name: cholecalciferol benzoate
• CAS No.: 2174-12-1
• Molecular Formula: C₃₄H₄₈O₂
• Molecular Weight: 488.754
• Mol file: 2174-12-1.mol

Synonyms:cholecalciferol benzoate

Chemical Property of cholecalciferol benzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cholecalciferol benzoate

There total 1 articles about cholecalciferol benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

vitamin D3 (67-97-0) + benzoyl chloride (98-88-4) → cholecalciferol benzoate (2174-12-1)

Guidance literature:

With pyridine;

DOI:10.1007/BF00777693

Reference yield:

cholecalciferol benzoate (2174-12-1) → vitamin D3 (67-97-0)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium sulfate

2: sodium hydroxide; methanol / 2.5 h / 25 - 30 °C / Large scale

With methanol; sodium sulfate; sodium hydroxide;

Reference yield:

cholecalciferol benzoate (2174-12-1) → C34H50O

Guidance literature:

With sodium sulfate;

upstream raw materials:

vitamin D₃

benzoyl chloride

Downstream raw materials:

(3S,10R,5Z,7E)-3-(Benzoyloxy)-19-hydroxy-9,10-secocholesta-5,7-diene

(3S,10S,5Z,7E)-3-(Benzoyloxy)-19-hydroxy-9,10-secocholesta-5,7-diene

(1S,4S,5Z,7E)-1-(Benzoyloxy)-4-acetoxy-A-homo-19-nor-9,10-secocholesta-5,7-diene

(1S,4R,5Z,7E)-1-(Benzoyloxy)-4-acetoxy-A-homo-19-nor-9,10-secocholesta-5,7-diene