3-(3-benzoyl-5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-tert-butoxycarbonylaminopropionic acid benzyl ester

Base Information

Chemical Name:3-(3-benzoyl-5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-tert-butoxycarbonylaminopropionic acid benzyl ester
CAS No.:573717-49-4
Molecular Formula:C₂₇H₂₉N₃O₇
Molecular Weight:507.543
Hs Code.:

Synonyms:3-(3-benzoyl-5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-tert-butoxycarbonylaminopropionic acid benzyl ester

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Chemical Property of 3-(3-benzoyl-5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-tert-butoxycarbonylaminopropionic acid benzyl ester

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Technology Process of 3-(3-benzoyl-5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-tert-butoxycarbonylaminopropionic acid benzyl ester

There total 3 articles about 3-(3-benzoyl-5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-tert-butoxycarbonylaminopropionic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 108957-20-6
(R)-N-(tert-butoxycarbonyl)-3-iodoalanine benzyl ester

: 4330-20-5
N-3-benzoylthymine

: 573717-49-4
3-(3-benzoyl-5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-tert-butoxycarbonylaminopropionic acid benzyl ester

: 244280-46-4
2-tert-butoxycarbonylamino-3-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)propionic acid benzyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1002/jhet.5570430445

Reference yield:

: 59524-02-6
N-tert-butoxycarbonyl-L-serine benzyl ester

: 573717-49-4
3-(3-benzoyl-5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-tert-butoxycarbonylaminopropionic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / -10 °C

2: NaI / acetone

3: 68 percent / K₂CO₃ / dimethylformamide / 12 h / 20 °C

With pyridine; potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; acetone;
DOI:10.1002/jhet.5570430445

Reference yield:

: 94882-74-3
benzyl 2(S)-(tert-butoxycarbonylamino)-3-p-toluenesulfonylpropionate

: 573717-49-4
3-(3-benzoyl-5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-tert-butoxycarbonylaminopropionic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaI / acetone

2: 68 percent / K₂CO₃ / dimethylformamide / 12 h / 20 °C

With potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; acetone;
DOI:10.1002/jhet.5570430445