C₅₄H₇₄N₆O₁₉

Base Information

Chemical Name:C₅₄H₇₄N₆O₁₉
CAS No.:622830-70-0
Molecular Formula:C₅₄H₇₄N₆O₁₉
Molecular Weight:1111.21
Hs Code.:

C<sub>54</sub>H<sub>74</sub>N<sub>6</sub>O<sub>19</sub>

Synonyms:C₅₄H₇₄N₆O₁₉

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Chemical Property of C₅₄H₇₄N₆O₁₉

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Technology Process of C₅₄H₇₄N₆O₁₉

There total 12 articles about C₅₄H₇₄N₆O₁₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 622830-69-7
C₆₉H₈₄N₆O₂₁

: 622830-70-0
C₅₄H₇₄N₆O₁₉

Guidance literature:: With piperidine; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 1h;
DOI:10.1021/jo034773s

Reference yield:

: 10022-13-6
1,3,4,6-tetra-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranose

: 622830-70-0
C₅₄H₇₄N₆O₁₉

Guidance literature:: Multi-step reaction with 10 steps

1.1: aq. HBr; AcOH / CH₂Cl₂ / 4 h / 20 °C

2.1: 75 percent / AgOTf; 4 Angstroem molecular sieves / CH₂Cl₂ / -40 - 20 °C

3.1: 87 percent / TBAF; AcOH / tetrahydrofuran / 72 h / 0 - 20 °C

4.1: 85 percent / CuBr₂; 4 Angstroem molecular sieves; Bu₄NBr / CH₂Cl₂; dimethylformamide / 20 °C

5.1: ethylenediamine / butan-1-ol / 90 °C

5.2: pyridine / 20 °C

5.3: 86 percent / NaOMe / methanol / 3 h / 20 °C

6.1: H₂ / Lindlar catalyst / methanol / 2.5 h / 20 °C

7.1: 132 mg / CH₂Cl₂ / 20 °C

8.1: 96 percent / H₂ / Pd(OH)2/C / methanol / 20 h / 20 °C

9.1: 1-methyl-pyrrolidin-2-one / 2 h / 20 °C

10.1: piperidine / 1-methyl-pyrrolidin-2-one / 1 h / 20 °C

With piperidine; 4 A molecular sieve; tetrabutyl ammonium fluoride; tetrabutylammomium bromide; hydrogen bromide; hydrogen; silver trifluoromethanesulfonate; acetic acid; ethylenediamine; copper(ll) bromide; palladium dihydroxide; Lindlar's catalyst; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; dichloromethane; N,N-dimethyl-formamide; butan-1-ol;
DOI:10.1021/jo034773s

Reference yield:

: 70831-94-6
3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-D-glucopyranosyl bromide

: 622830-70-0
C₅₄H₇₄N₆O₁₉

Guidance literature:: Multi-step reaction with 9 steps

1.1: 75 percent / AgOTf; 4 Angstroem molecular sieves / CH₂Cl₂ / -40 - 20 °C

2.1: 87 percent / TBAF; AcOH / tetrahydrofuran / 72 h / 0 - 20 °C

3.1: 85 percent / CuBr₂; 4 Angstroem molecular sieves; Bu₄NBr / CH₂Cl₂; dimethylformamide / 20 °C

4.1: ethylenediamine / butan-1-ol / 90 °C

4.2: pyridine / 20 °C

4.3: 86 percent / NaOMe / methanol / 3 h / 20 °C

5.1: H₂ / Lindlar catalyst / methanol / 2.5 h / 20 °C

6.1: 132 mg / CH₂Cl₂ / 20 °C

7.1: 96 percent / H₂ / Pd(OH)2/C / methanol / 20 h / 20 °C

8.1: 1-methyl-pyrrolidin-2-one / 2 h / 20 °C

9.1: piperidine / 1-methyl-pyrrolidin-2-one / 1 h / 20 °C

With piperidine; 4 A molecular sieve; tetrabutyl ammonium fluoride; tetrabutylammomium bromide; hydrogen; silver trifluoromethanesulfonate; acetic acid; ethylenediamine; copper(ll) bromide; palladium dihydroxide; Lindlar's catalyst; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; dichloromethane; N,N-dimethyl-formamide; butan-1-ol;
DOI:10.1021/jo034773s