Technology Process of (Z)-3-(4-nitrophenyl)-3-phenylacrylaldehyde
There total 6 articles about (Z)-3-(4-nitrophenyl)-3-phenylacrylaldehyde which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Dess-Martin periodane;
In
dichloromethane;
at 20 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C
1.2: Reflux
2.1: potassium carbonate; methanol / 1 h / Reflux
3.1: borane-THF / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere
4.1: Dess-Martin periodane / dichloromethane / 20 °C / Inert atmosphere
With
methanol; borane-THF; sodium hydride; potassium carbonate; Dess-Martin periodane;
In
tetrahydrofuran; dichloromethane; mineral oil;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate; methanol / 1 h / Reflux
2: borane-THF / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere
3: Dess-Martin periodane / dichloromethane / 20 °C / Inert atmosphere
With
methanol; borane-THF; potassium carbonate; Dess-Martin periodane;
In
tetrahydrofuran; dichloromethane;
