4-amino-2'-methyl-4'-nitrodiphenyl sulfide

Base Information

Chemical Name:4-amino-2'-methyl-4'-nitrodiphenyl sulfide
CAS No.:176512-30-4
Molecular Formula:C₂₃H₂₃BrN₂O₄S₂
Molecular Weight:535.483
Hs Code.:

4-<N-(3-bromopropyl)-N-tosyl>amino-2'-methyl-4'-nitrodiphenyl sulfide

Synonyms:4-amino-2'-methyl-4'-nitrodiphenyl sulfide

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Chemical Property of 4-amino-2'-methyl-4'-nitrodiphenyl sulfide

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Technology Process of 4-amino-2'-methyl-4'-nitrodiphenyl sulfide

There total 3 articles about 4-amino-2'-methyl-4'-nitrodiphenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 109-64-8
1,3-dibromo-propane

: 176512-25-7
4-Methyl-N-[4-(2-methyl-4-nitro-phenylsulfanyl)-phenyl]-benzenesulfonamide

: 176512-30-4
4-amino-2'-methyl-4'-nitrodiphenyl sulfide

Guidance literature:: With potassium hydroxide; copper(l) iodide; sodium iodide; In ethanol; for 17h; Heating;
DOI:10.1002/ardp.19963290309

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 176512-30-4
4-amino-2'-methyl-4'-nitrodiphenyl sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 3 h

2: 79 percent / NaI, CuI, aq. KOH / ethanol / 17 h / Heating

With potassium hydroxide; copper(l) iodide; sodium iodide; In pyridine; ethanol;
DOI:10.1002/ardp.19963290309

Reference yield:

: 4-(2-Methyl-4-nitro-phenylsulfanyl)-phenylamine

: 176512-30-4
4-amino-2'-methyl-4'-nitrodiphenyl sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 3 h

2: 79 percent / NaI, CuI, aq. KOH / ethanol / 17 h / Heating

With potassium hydroxide; copper(l) iodide; sodium iodide; In pyridine; ethanol;
DOI:10.1002/ardp.19963290309