methoxycarbonylmethyl 6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

Base Information

Chemical Name:methoxycarbonylmethyl 6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside
CAS No.:441017-72-7
Molecular Formula:C₅₉H₆₄O₁₃S
Molecular Weight:1013.22
Hs Code.:

Synonyms:methoxycarbonylmethyl 6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

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Chemical Property of methoxycarbonylmethyl 6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

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Technology Process of methoxycarbonylmethyl 6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

There total 5 articles about methoxycarbonylmethyl 6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 441017-58-9
6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl iodide

: 441017-65-8
methoxycarbonylmethyl 2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

: 441017-72-7
methoxycarbonylmethyl 6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

Guidance literature:: With 4 A molecular sieve; tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; In benzene; for 4h; Heating;
DOI:10.1021/ol025887d

Reference yield: 88.0%

: 441017-58-9
6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl iodide

: 441017-65-8
methoxycarbonylmethyl 2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

: 1,5-anhydro-6-O-acetyl-2,3,4-tri-O-benzyl-D-arabino-hex-1-enitol

: 441017-72-7
methoxycarbonylmethyl 6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

Guidance literature:: With tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; In benzene; for 4h; Heating;

Reference yield:

: 3879-79-6,17791-37-6,19488-61-0,53008-63-2,61330-62-9,69237-94-1,69237-95-2,71526-33-5,83462-67-3,84799-77-9,103421-29-0,103421-30-3,139241-42-2
methyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

: 441017-72-7
methoxycarbonylmethyl 6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: ZnCl₂ / acetic acid / 4 h / 20 °C

2: 100 percent / iodo trimethylsilane / CH₂Cl₂ / 2 h / 0 °C

3: 88 percent / tetrabutylammonium idide; diisopropylethylamine / benzene / 4 h / Heating

With trimethylsilyl iodide; tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; zinc(II) chloride; In dichloromethane; acetic acid; benzene;