t-butyl 2-phenoxypropanothioate

Base Information

• Chemical Name: t-butyl 2-phenoxypropanothioate
• CAS No.: 29279-27-4
• Molecular Formula: C₁₃H₁₈O₂S
• Molecular Weight: 238.351
• Mol file: 29279-27-4.mol

Synonyms:t-butyl 2-phenoxypropanothioate

Chemical Property of t-butyl 2-phenoxypropanothioate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of t-butyl 2-phenoxypropanothioate

There total 1 articles about t-butyl 2-phenoxypropanothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2-phenoxypropionic acid (940-31-8) + 2-methylpropan-2-thiol (75-66-1) → t-butyl 2-phenoxypropanothioate (29279-27-4)

Guidance literature:

With pyridine; O-phenyl phosphorodichloridate; In 1,2-dimethoxyethane; for 16h; Ambient temperature;

Reference yield: 99.0%

t-butyl 2-phenoxypropanothioate (29279-27-4) → 2-phenoxy-1-propanol (4169-04-4)

Guidance literature:

With sodium tetrahydroborate; In ethanol; for 24h; Ambient temperature;

Reference yield:

t-butyl 2-phenoxypropanothioate (29279-27-4) + isopropyl alcohol (67-63-0,8013-70-5) → 2-phenoxy-1-propanol (4169-04-4) + isopropyl 2-phenoxypropanoate

Guidance literature:

With sodium tetrahydroborate; for 22h; Yield given. Yields of byproduct given; Ambient temperature;

upstream raw materials:

2-phenoxypropionic acid

2-methylpropan-2-thiol

Downstream raw materials:

2-phenoxy-1-propanol