2-(6,11-Dihydrodibenzo(b,e)thiepin-11-ylamino)acetamide

Base Information

Chemical Name:2-(6,11-Dihydrodibenzo(b,e)thiepin-11-ylamino)acetamide
CAS No.:117125-44-7
Molecular Formula:C₁₆H₁₆N₂OS
Molecular Weight:284.382
Hs Code.:
DSSTox Substance ID:DTXSID60922299
Mol file:117125-44-7.mol

Synonyms:BRN 4492798;2-(6,11-Dihydrodibenzo(b,e)thiepin-11-ylamino)acetamide;117125-44-7;Acetamide, 2-((6,11-dihydrodibenzo(b,e)thiepin-11-yl)amino)-;SCHEMBL9691458;DTXSID60922299;LS-9165;2-[(6,11-Dihydrodibenzo[b,e]thiepin-11-yl)amino]ethanimidic acid

Suppliers and Price of 2-(6,11-Dihydrodibenzo(b,e)thiepin-11-ylamino)acetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(6,11-Dihydrodibenzo(b,e)thiepin-11-ylamino)acetamide

Chemical Property:

Vapor Pressure:6.31E-10mmHg at 25°C
Boiling Point:494.7°Cat760mmHg
Flash Point:253°C
Density:1.29g/cm³
XLogP3:2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:284.09833431
Heavy Atom Count:20
Complexity:349

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C2=CC=CC=C2C(C3=CC=CC=C3S1)NCC(=O)N

Technology Process of 2-(6,11-Dihydrodibenzo(b,e)thiepin-11-ylamino)acetamide

There total 3 articles about 2-(6,11-Dihydrodibenzo(b,e)thiepin-11-ylamino)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 117125-39-0
ethyl 2-(6,11-dihydrodibenzothiepin-11-ylamino)acetate

: 117125-44-7
2-(6,11-dihydrodibenzothiepin-11-ylamino)acetamide

Guidance literature:: With ammonia; In methanol; at 135 ℃; for 4h; high pressure;

Reference yield:

: hydrochloride monohydrate

: 1725-29-7
2,3-5,6-dibenzo-4-thiacycloheptanylamine

: 144-48-9
iodacetamide

: 117125-44-7
2-(6,11-dihydrodibenzothiepin-11-ylamino)acetamide

Guidance literature:: In ethanol; dichloromethane; sodium hydrogencarbonate; ethyl acetate; isopropyl alcohol; pentane;

Reference yield:

: 1745-53-5
11-amino-6,11-dihydrodibenzothiepin

: 117125-44-7
2-(6,11-dihydrodibenzothiepin-11-ylamino)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / K₂CO₃ / toluene / 32 h / Heating

2: 94 percent / NH₃(l) / methanol / 4 h / 135 °C / high pressure

With ammonia; potassium carbonate; In methanol; toluene;