2,4-Dichlorocinnamylchloride

Base Information

Chemical Name:2,4-Dichlorocinnamylchloride
CAS No.:77975-44-1
Molecular Formula:C₉H₇Cl₃
Molecular Weight:221.514
Hs Code.:
DSSTox Substance ID:DTXSID501246195

Synonyms:2,4-dichlorocinnamylchloride;AFLBPVZOGNDRFH-UHFFFAOYSA-N;DTXSID501246195;AKOS017887756;77975-44-1;2,4-Dichloro-1-(3-chloro-1-propen-1-yl)benzene

Suppliers and Price of 2,4-Dichlorocinnamylchloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2,4-Dichlorocinnamylchloride

Chemical Property:

XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:219.961333
Heavy Atom Count:12
Complexity:156

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=C(C=C1Cl)Cl)C=CCCl

Technology Process of 2,4-Dichlorocinnamylchloride

There total 6 articles about 2,4-Dichlorocinnamylchloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 148775-23-9
(2E)-3-(2,4-dichlorophenyl)prop-2-en-1-ol

: 77975-44-1
1-Chloro-3-(2,4-dichlorophenyl)prop-2-ene

Guidance literature:: With pyridine; thionyl chloride; In benzene; for 84h; Ambient temperature;
DOI:10.1021/jm00364a024

Reference yield:

: 1201-99-6,20595-45-3,20595-46-4
trans-2,4-dichlorocinnamic acid

: 77975-44-1
1-Chloro-3-(2,4-dichlorophenyl)prop-2-ene

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride, pyridine / 40 °C

2: sodium borohydride / dioxane / Ambient temperature

3: thionyl chloride, pyridine / benzene / 84 h / Ambient temperature

With pyridine; sodium tetrahydroborate; thionyl chloride; In 1,4-dioxane; benzene;
DOI:10.1021/jm00364a024

Reference yield:

: 82476-04-8
(E)-3-(2,4-dichlorophenyl)acryloyl chloride

: 77975-44-1
1-Chloro-3-(2,4-dichlorophenyl)prop-2-ene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium borohydride / dioxane / Ambient temperature

2: thionyl chloride, pyridine / benzene / 84 h / Ambient temperature

With pyridine; sodium tetrahydroborate; thionyl chloride; In 1,4-dioxane; benzene;
DOI:10.1021/jm00364a024