methyl 2,3,6-tri-O-benzyl-4-O-(methylthio)thiocarbonyl-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2,3,6-tri-O-benzyl-4-O-(methylthio)thiocarbonyl-α-D-glucopyranoside
CAS No.:160533-92-6
Molecular Formula:C₃₀H₃₄O₆S₂
Molecular Weight:554.728
Hs Code.:

Synonyms:methyl 2,3,6-tri-O-benzyl-4-O-(methylthio)thiocarbonyl-α-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2,3,6-tri-O-benzyl-4-O-(methylthio)thiocarbonyl-α-D-glucopyranoside

Chemical Property:

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Technology Process of methyl 2,3,6-tri-O-benzyl-4-O-(methylthio)thiocarbonyl-α-D-glucopyranoside

There total 1 articles about methyl 2,3,6-tri-O-benzyl-4-O-(methylthio)thiocarbonyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 19488-48-3
methyl O-2,3,6-tri-O-benzyl-α-D-glucopyranoside

: 74-88-4
methyl iodide

: 160533-92-6
methyl 2,3,6-tri-O-benzyl-4-O-(methylthio)thiocarbonyl-α-D-glucopyranoside

Guidance literature:: With 1H-imidazole; sodium hydride; Yield given. Multistep reaction;
DOI:10.1016/0008-6215(94)84006-7

Reference yield: 95.0%

: 160533-92-6
methyl 2,3,6-tri-O-benzyl-4-O-(methylthio)thiocarbonyl-α-D-glucopyranoside

: 87871-04-3
methyl 2,3,6-tri-O-benzyl-4-deoxy-α-D-xylo-hexopyranoside

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 1.5h; Heating;
DOI:10.1016/0008-6215(94)84006-7

Reference yield:

: 160533-92-6
methyl 2,3,6-tri-O-benzyl-4-O-(methylthio)thiocarbonyl-α-D-glucopyranoside

: 2,3,6-tri-O-benzyl-4-deoxy-D-xylo-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / azobis(isobutyronitrile), tributyltin hydride / toluene / 1.5 h / Heating

2: 80 percent / AcOH, HCl / 4.5 h / 80 °C

With hydrogenchloride; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; acetic acid; In toluene;
DOI:10.1016/0008-6215(94)84006-7