3,4-di-O-acetyl-α-1-O-benzyl-6-O-p-methylbenzenesulfonate-N-acetylglucosamine

Base Information

Chemical Name:3,4-di-O-acetyl-α-1-O-benzyl-6-O-p-methylbenzenesulfonate-N-acetylglucosamine
CAS No.:61891-77-8
Molecular Formula:C₂₆H₃₁NO₁₀S
Molecular Weight:549.599
Hs Code.:

Synonyms:3,4-di-O-acetyl-α-1-O-benzyl-6-O-p-methylbenzenesulfonate-N-acetylglucosamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-di-O-acetyl-α-1-O-benzyl-6-O-p-methylbenzenesulfonate-N-acetylglucosamine

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Technology Process of 3,4-di-O-acetyl-α-1-O-benzyl-6-O-p-methylbenzenesulfonate-N-acetylglucosamine

There total 6 articles about 3,4-di-O-acetyl-α-1-O-benzyl-6-O-p-methylbenzenesulfonate-N-acetylglucosamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 58902-18-4
α-1-O-benzyl-6-O-p-methylbenzenesulfonate-N-acetylglucosamine

: 108-24-7
acetic anhydride

: 61891-77-8
3,4-di-O-acetyl-α-1-O-benzyl-6-O-p-methylbenzenesulfonate-N-acetylglucosamine

Guidance literature:: With pyridine; at 20 ℃; for 3h;
DOI:10.1021/ja504063c

Reference yield:

: 7512-17-6,72-87-7,1136-42-1,1136-44-3,6082-29-7,6730-06-9,7772-94-3,10036-64-3,14131-60-3,14131-64-7,14131-68-1,14215-68-0,62057-49-2,62057-50-5,62057-51-6,62057-52-7,62057-53-8,62057-54-9,62057-55-0,62057-56-1,62075-50-7,62137-54-6,134451-97-1,134522-12-6,148347-16-4
N-Acetyl-D-glucosamine

: 61891-77-8
3,4-di-O-acetyl-α-1-O-benzyl-6-O-p-methylbenzenesulfonate-N-acetylglucosamine

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / water / 4 h / 75 °C

2: pyridine / 1 h / -20 °C / Inert atmosphere

3: pyridine / 3 h / 20 °C

With pyridine; hydrogenchloride; In water;
DOI:10.1021/ja504063c

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 61891-77-8
3,4-di-O-acetyl-α-1-O-benzyl-6-O-p-methylbenzenesulfonate-N-acetylglucosamine

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / water / 4 h / 75 °C

2: pyridine / 1 h / -20 °C / Inert atmosphere

3: pyridine / 3 h / 20 °C

With pyridine; hydrogenchloride; In water;
DOI:10.1021/ja504063c