2-acetamido-3,4,-di-O-acetyl-2-deoxy2-6-O-tosyl-α-D-glucopyranose 1-dibenzylphosphate

Base Information

Chemical Name:2-acetamido-3,4,-di-O-acetyl-2-deoxy2-6-O-tosyl-α-D-glucopyranose 1-dibenzylphosphate
CAS No.:1280709-58-1
Molecular Formula:C₃₃H₃₈NO₁₃PS
Molecular Weight:719.703
Hs Code.:

Synonyms:2-acetamido-3,4,-di-O-acetyl-2-deoxy2-6-O-tosyl-α-D-glucopyranose 1-dibenzylphosphate

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Chemical Property of 2-acetamido-3,4,-di-O-acetyl-2-deoxy2-6-O-tosyl-α-D-glucopyranose 1-dibenzylphosphate

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Technology Process of 2-acetamido-3,4,-di-O-acetyl-2-deoxy2-6-O-tosyl-α-D-glucopyranose 1-dibenzylphosphate

There total 9 articles about 2-acetamido-3,4,-di-O-acetyl-2-deoxy2-6-O-tosyl-α-D-glucopyranose 1-dibenzylphosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₃₈NO₁₂PS

: 1280709-58-1
2-acetamido-3,4,-di-O-acetyl-2-deoxy2-6-O-tosyl-α-D-glucopyranose 1-dibenzylphosphate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 - 20 ℃;
DOI:10.1016/j.bmcl.2010.12.090

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1280709-58-1
2-acetamido-3,4,-di-O-acetyl-2-deoxy2-6-O-tosyl-α-D-glucopyranose 1-dibenzylphosphate

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 6.5 h / 0 °C / Inert atmosphere

2: 20 °C

3: 20 % Pd(OH)2/C; hydrogen / methanol / 48 h / 2585.81 Torr

4: 1H-tetrazole / dichloromethane / 1.5 h / 20 °C

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -78 - 20 °C

With pyridine; 1H-tetrazole; 20 % Pd(OH)2/C; hydrogen; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane;
DOI:10.1016/j.bmcl.2010.12.090

Reference yield:

: 13343-62-9,347411-88-5
benzyl 2-acetamido-2-deoxy-α-D-glucopyranoside

: 1280709-58-1
2-acetamido-3,4,-di-O-acetyl-2-deoxy2-6-O-tosyl-α-D-glucopyranose 1-dibenzylphosphate

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 6.5 h / 0 °C / Inert atmosphere

2: 20 °C

3: 20 % Pd(OH)2/C; hydrogen / methanol / 48 h / 2585.81 Torr

4: 1H-tetrazole / dichloromethane / 1.5 h / 20 °C

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -78 - 20 °C

With pyridine; 1H-tetrazole; 20 % Pd(OH)2/C; hydrogen; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane;
DOI:10.1016/j.bmcl.2010.12.090