4,6-O-benzylideneglucosaminylglycyl-alanyl-4,6-O-benzylideneglucosaminylglycylalanyl amide acetic acid salt

Base Information

Chemical Name:4,6-O-benzylideneglucosaminylglycyl-alanyl-4,6-O-benzylideneglucosaminylglycylalanyl amide acetic acid salt
CAS No.:79943-67-2
Molecular Formula:C₂H₄O₂*C₃₆H₄₉N₇O₁₄
Molecular Weight:863.876
Hs Code.:

Synonyms:4,6-O-benzylideneglucosaminylglycyl-alanyl-4,6-O-benzylideneglucosaminylglycylalanyl amide acetic acid salt

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Chemical Property of 4,6-O-benzylideneglucosaminylglycyl-alanyl-4,6-O-benzylideneglucosaminylglycylalanyl amide acetic acid salt

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Technology Process of 4,6-O-benzylideneglucosaminylglycyl-alanyl-4,6-O-benzylideneglucosaminylglycylalanyl amide acetic acid salt

There total 10 articles about 4,6-O-benzylideneglucosaminylglycyl-alanyl-4,6-O-benzylideneglucosaminylglycylalanyl amide acetic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 64-19-7,77671-22-8
acetic acid

: 79943-63-8
Z-4,6-O-benzylideneglucosaminylglycylalanyl-4,6-O-benzylideneglucosaminylglycylalanine amide

: 79943-67-2
4,6-O-benzylideneglucosaminylglycyl-alanyl-4,6-O-benzylideneglucosaminylglycylalanyl amide acetic acid salt

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide; at 25 ℃;

Reference yield:

: 40149-87-9
Z-4,6-O-benzylideneglucosaminyl hydrazide

: 79943-67-2
4,6-O-benzylideneglucosaminylglycyl-alanyl-4,6-O-benzylideneglucosaminylglycylalanyl amide acetic acid salt

Guidance literature:: Multi-step reaction with 5 steps

1: 6 N HCl, NaNO₂ / dimethylformamide; H₂O

2: triethylamine / H₂O; dimethylformamide / 1.) 0 deg C, 1 h, 2.) 1 h, RT, 3.) 16 h

3: 93 percent / H₂ / 10 percent Pd/C / methanol / 6 h

4: triethylamine / dimethylformamide / 1.) 0 deg C, 1 h, 2.) 1 h, RT, 3.) 16 h

5: 91 percent / H₂ / 10 percent Pd/C / dimethylformamide; methanol / 25 °C

With hydrogenchloride; hydrogen; triethylamine; sodium nitrite; palladium on activated charcoal; In methanol; water; N,N-dimethyl-formamide;

Reference yield:

: 77437-40-2
Z-BEGA-N₃

: 79943-67-2
4,6-O-benzylideneglucosaminylglycyl-alanyl-4,6-O-benzylideneglucosaminylglycylalanyl amide acetic acid salt

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / H₂O; dimethylformamide / 1.) 0 deg C, 1 h, 2.) 1 h, RT, 3.) 16 h

2: 93 percent / H₂ / 10 percent Pd/C / methanol / 6 h

3: triethylamine / dimethylformamide / 1.) 0 deg C, 1 h, 2.) 1 h, RT, 3.) 16 h

4: 91 percent / H₂ / 10 percent Pd/C / dimethylformamide; methanol / 25 °C

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; water; N,N-dimethyl-formamide;