3-(4-allyl-4-methyl-5-oxo-tetrahydro-furan-3-yl)-3-phenyl-propionaldehyde

Base Information

Chemical Name:3-(4-allyl-4-methyl-5-oxo-tetrahydro-furan-3-yl)-3-phenyl-propionaldehyde
CAS No.:332940-63-3
Molecular Formula:C₁₇H₂₀O₃
Molecular Weight:272.344
Hs Code.:

Synonyms:3-(4-allyl-4-methyl-5-oxo-tetrahydro-furan-3-yl)-3-phenyl-propionaldehyde

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Chemical Property of 3-(4-allyl-4-methyl-5-oxo-tetrahydro-furan-3-yl)-3-phenyl-propionaldehyde

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Technology Process of 3-(4-allyl-4-methyl-5-oxo-tetrahydro-furan-3-yl)-3-phenyl-propionaldehyde

There total 2 articles about 3-(4-allyl-4-methyl-5-oxo-tetrahydro-furan-3-yl)-3-phenyl-propionaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 332940-61-1
[(Z)-(S)-3-((3S,4S)-4-Allyl-4-methyl-5-oxo-tetrahydro-furan-3-yl)-3-phenyl-propenyl]-(4-methoxy-phenyl)-carbamic acid tert-butyl ester

: 332940-63-3
3-(4-allyl-4-methyl-5-oxo-tetrahydro-furan-3-yl)-3-phenyl-propionaldehyde

Guidance literature:: With hydrogenchloride; In chloroform;
DOI:10.1021/ol007012+

Reference yield:

: 332940-45-1
(4-Methoxy-phenyl)-[(Z)-(S)-3-((3S,4S)-4-methyl-5-oxo-tetrahydro-furan-3-yl)-3-phenyl-propenyl]-carbamic acid tert-butyl ester

: 332940-63-3
3-(4-allyl-4-methyl-5-oxo-tetrahydro-furan-3-yl)-3-phenyl-propionaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: LDA / tetrahydrofuran / -78 °C

1.2: tetrahydrofuran

2.1: 77 percent / aq. HCl / CHCl₃

With hydrogenchloride; lithium diisopropyl amide; In tetrahydrofuran; chloroform;
DOI:10.1021/ol007012+

Reference yield: 73.0%

: 1779-49-3
Methyltriphenylphosphonium bromide

: 332940-63-3
3-(4-allyl-4-methyl-5-oxo-tetrahydro-furan-3-yl)-3-phenyl-propionaldehyde

: 332940-65-5
3-allyl-3-methyl-4-(1-phenyl-but-3-enyl)-dihydro-furan-2-one

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; at -78 ℃;

3-(4-allyl-4-methyl-5-oxo-tetrahydro-furan-3-yl)-3-phenyl-propionaldehyde; In tetrahydrofuran; Further stages.;
DOI:10.1021/ol007012+