(5E)-3-O-benzoyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-xylo-hexofuran-5-enose

Base Information

Chemical Name:(5E)-3-O-benzoyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-xylo-hexofuran-5-enose
CAS No.:124572-44-7
Molecular Formula:C₃₅H₃₂O₆
Molecular Weight:548.635
Hs Code.:

Synonyms:(5E)-3-O-benzoyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-xylo-hexofuran-5-enose

Suppliers and Price of (5E)-3-O-benzoyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-xylo-hexofuran-5-enose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (5E)-3-O-benzoyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-xylo-hexofuran-5-enose

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (5E)-3-O-benzoyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-xylo-hexofuran-5-enose

There total 1 articles about (5E)-3-O-benzoyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-xylo-hexofuran-5-enose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 613-90-1
benzoyl cyanide

: 4056-10-4
1,2-O-Isopropyliden-6-O-triphenylmethyl-5-desoxy-α-D-xylo-hexofuran-5-enose

: 124572-44-7
(5E)-3-O-benzoyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-xylo-hexofuran-5-enose

Guidance literature:: With triethylamine; In 1,4-dioxane; for 1h; Ambient temperature;

Reference yield:

: 124572-44-7
(5E)-3-O-benzoyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-xylo-hexofuran-5-enose

: 113808-31-4
Benzoic acid (2R,3R,4R,5R)-4-acetoxy-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-(2-phosphono-ethyl)-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 12 steps

1: acetic acid / dioxane; H₂O / 0.75 h / Heating

2: sodium borohydride / ethanol / 0.25 h / Ambient temperature

3: 95 percent / pyridine / 24 h / 20 °C

4: 97 percent / sodium methylate / methanol / 0.5 h / Ambient temperature

5: 1)dimethyl sulfoxide/acetic anhydride, 2)sodium borohydride / 1)1.5h, 70 deg C, 2)1h, room temperature

6: 85 percent / triethylamine / dioxane / 1 h / 20 °C

7: 89 percent / tin tetrachloride / 1,2-dichloro-ethane / 0.08 h / 20 °C

8: 78 percent / triphenylphosphine/carbon tetrabromide / dimethylformamide / 16 h / 20 °C

9: 100 percent / 4 h / Heating

10: sulfuric acid / acetic acid / 18 h / 20 °C

11: 30 percent / trimethylsilyl trifluoromethanesulfonate / 1,2-dichloro-ethane / 16 h / 20 °C

12: bromotrimethylsilane / 1,2-dichloro-ethane / 16 h / 20 °C

With sodium tetrahydroborate; trimethylsilyl bromide; carbon tetrabromide; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; sodium methylate; acetic anhydride; tin(IV) chloride; acetic acid; dimethyl sulfoxide; triethylamine; triphenylphosphine; In 1,4-dioxane; pyridine; methanol; ethanol; water; acetic acid; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 124572-44-7
(5E)-3-O-benzoyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-xylo-hexofuran-5-enose

: 113808-29-0
1-(2-O-acetyl-3-O-benzoyl-5,6-dideoxy-6-diethylphosphono-β-D-ribo-hexofuranosyl)uracil

Guidance literature:: Multi-step reaction with 11 steps

1: acetic acid / dioxane; H₂O / 0.75 h / Heating

2: sodium borohydride / ethanol / 0.25 h / Ambient temperature

3: 95 percent / pyridine / 24 h / 20 °C

4: 97 percent / sodium methylate / methanol / 0.5 h / Ambient temperature

5: 1)dimethyl sulfoxide/acetic anhydride, 2)sodium borohydride / 1)1.5h, 70 deg C, 2)1h, room temperature

6: 85 percent / triethylamine / dioxane / 1 h / 20 °C

7: 89 percent / tin tetrachloride / 1,2-dichloro-ethane / 0.08 h / 20 °C

8: 78 percent / triphenylphosphine/carbon tetrabromide / dimethylformamide / 16 h / 20 °C

9: 100 percent / 4 h / Heating

10: sulfuric acid / acetic acid / 18 h / 20 °C

11: 30 percent / trimethylsilyl trifluoromethanesulfonate / 1,2-dichloro-ethane / 16 h / 20 °C

With sodium tetrahydroborate; carbon tetrabromide; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; sodium methylate; acetic anhydride; tin(IV) chloride; acetic acid; dimethyl sulfoxide; triethylamine; triphenylphosphine; In 1,4-dioxane; pyridine; methanol; ethanol; water; acetic acid; 1,2-dichloro-ethane; N,N-dimethyl-formamide;