C₂₄H₁₉ClF₂N₄O₄

Base Information

Chemical Name:C₂₄H₁₉ClF₂N₄O₄
CAS No.:1622205-49-5
Molecular Formula:C₂₄H₁₉ClF₂N₄O₄
Molecular Weight:500.889
Hs Code.:

C<sub>24</sub>H<sub>19</sub>ClF<sub>2</sub>N<sub>4</sub>O<sub>4</sub>

Synonyms:C₂₄H₁₉ClF₂N₄O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₁₉ClF₂N₄O₄

Chemical Property:

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Technology Process of C₂₄H₁₉ClF₂N₄O₄

There total 10 articles about C₂₄H₁₉ClF₂N₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 139-85-5
3,4-dihydroxybenzaldehyde

: 1622205-49-5
C₂₄H₁₉ClF₂N₄O₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium hydroxide / water; N,N-dimethyl-formamide / 2 h / 120 °C

2.1: potassium carbonate / acetonitrile / 3 h / 20 °C

3.1: acetic acid; ammonium acetate / 3 h / 130 °C / Inert atmosphere

4.1: acetic acid; nitric acid / dichloromethane / 3.92 h / 75 °C / Cooling with ice

4.2: 1 h / 70 °C / Inert atmosphere

5.1: palladium 10% on activated carbon; hydrogen / water; ethanol / 1.25 h / 20 °C

6.1: acetic acid; potassium tert-butylate / dimethyl sulfoxide / 1.33 h / 160 °C / Inert atmosphere

7.1: methanol; sodium methylate / 3.5 h / 65 °C / Inert atmosphere

8.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C / Inert atmosphere

8.2: 0.83 h / 0 - 20 °C / Inert atmosphere

9.1: triethylamine / tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere

With methanol; palladium 10% on activated carbon; potassium tert-butylate; ammonium acetate; hydrogen; nitric acid; sodium methylate; sodium hydride; potassium carbonate; acetic acid; triethylamine; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile; mineral oil;

Reference yield:

: 1622205-53-1
6-(difluoromethoxy)-1H-indol-5-ol

: 1622205-49-5
C₂₄H₁₉ClF₂N₄O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid; potassium tert-butylate / dimethyl sulfoxide / 1.33 h / 160 °C / Inert atmosphere

2.1: methanol; sodium methylate / 3.5 h / 65 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C / Inert atmosphere

3.2: 0.83 h / 0 - 20 °C / Inert atmosphere

4.1: triethylamine / tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere

With methanol; potassium tert-butylate; sodium methylate; sodium hydride; acetic acid; triethylamine; In tetrahydrofuran; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 151103-08-1
4-difluoromethoxy-3-hydroxybenzaldehyde

: 1622205-49-5
C₂₄H₁₉ClF₂N₄O₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium carbonate / acetonitrile / 3 h / 20 °C

2.1: acetic acid; ammonium acetate / 3 h / 130 °C / Inert atmosphere

3.1: acetic acid; nitric acid / dichloromethane / 3.92 h / 75 °C / Cooling with ice

3.2: 1 h / 70 °C / Inert atmosphere

4.1: palladium 10% on activated carbon; hydrogen / water; ethanol / 1.25 h / 20 °C

5.1: acetic acid; potassium tert-butylate / dimethyl sulfoxide / 1.33 h / 160 °C / Inert atmosphere

6.1: methanol; sodium methylate / 3.5 h / 65 °C / Inert atmosphere

7.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C / Inert atmosphere

7.2: 0.83 h / 0 - 20 °C / Inert atmosphere

8.1: triethylamine / tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere

With methanol; palladium 10% on activated carbon; potassium tert-butylate; ammonium acetate; hydrogen; nitric acid; sodium methylate; sodium hydride; potassium carbonate; acetic acid; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile; mineral oil;