N-benzoyl-3',5'-di-O-levulinoyl-β-L-2'-deoxycytidine

Base Information

Chemical Name:N-benzoyl-3',5'-di-O-levulinoyl-β-L-2'-deoxycytidine
CAS No.:793717-03-0
Molecular Formula:C₂₆H₂₉N₃O₉
Molecular Weight:527.531
Hs Code.:

Synonyms:N-benzoyl-3',5'-di-O-levulinoyl-β-L-2'-deoxycytidine

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Chemical Property of N-benzoyl-3',5'-di-O-levulinoyl-β-L-2'-deoxycytidine

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Technology Process of N-benzoyl-3',5'-di-O-levulinoyl-β-L-2'-deoxycytidine

There total 1 articles about N-benzoyl-3',5'-di-O-levulinoyl-β-L-2'-deoxycytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 123-76-2
levulinic acid

: 189074-86-0
N-benzoyl-β-L-2'-deoxycytidine

: 793717-03-0
N-benzoyl-3',5'-di-O-levulinoyl-β-L-2'-deoxycytidine

Guidance literature:: With dmap; triethylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane; at 20 ℃; for 2h;
DOI:10.1021/ol048502v

Reference yield: 80.0%

: 793717-03-0
N-benzoyl-3',5'-di-O-levulinoyl-β-L-2'-deoxycytidine

: 189074-86-0
N-benzoyl-β-L-2'-deoxycytidine

: N-benzoyl-3'-O-levulinoyl-β-L-2'-deoxycytidine

Guidance literature:: With phosphate buffer; Chromobacterium viscosum; In 1,4-dioxane; at 30 ℃; for 25.5h; pH=7;
DOI:10.1021/ol048502v

Reference yield:

: 793717-03-0
N-benzoyl-3',5'-di-O-levulinoyl-β-L-2'-deoxycytidine

: N-benzoyl-5'-O-levulinoyl-2'-deoxy-β-L-cytidine

Guidance literature:: Multi-step reaction with 2 steps

1: 13 percent Spectr_. / phosphate buffer; Chromobacterium viscosum / dioxane / 25.5 h / 30 °C / pH 7

2: 88 percent / Candida antarctica lipase B / tetrahydrofuran / 2 h / 30 °C / Enzymatic reaction

With Candida antarctica lipase B; phosphate buffer; Chromobacterium viscosum; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1021/ol048502v