(3R,4R)-1-(chrysen-6-yl)-3-hydroxy-4-(4-methoxyphenyl)azetidin-2-oneacetate

Base Information

Chemical Name:(3R,4R)-1-(chrysen-6-yl)-3-hydroxy-4-(4-methoxyphenyl)azetidin-2-oneacetate
CAS No.:1215310-74-9
Molecular Formula:C₂₉H₂₁NO₃
Molecular Weight:431.491
Hs Code.:

Synonyms:(3R,4R)-1-(chrysen-6-yl)-3-hydroxy-4-(4-methoxyphenyl)azetidin-2-oneacetate

Suppliers and Price of (3R,4R)-1-(chrysen-6-yl)-3-hydroxy-4-(4-methoxyphenyl)azetidin-2-oneacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R,4R)-1-(chrysen-6-yl)-3-hydroxy-4-(4-methoxyphenyl)azetidin-2-oneacetate

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Technology Process of (3R,4R)-1-(chrysen-6-yl)-3-hydroxy-4-(4-methoxyphenyl)azetidin-2-oneacetate

There total 4 articles about (3R,4R)-1-(chrysen-6-yl)-3-hydroxy-4-(4-methoxyphenyl)azetidin-2-oneacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1215310-72-7
(3R,4R)-1-(chrysen-6-yl)-3-hydroxy-4-phenylazetidin-2-one

: 75-36-5
acetyl chloride

: 1215310-74-9,302595-58-0
(3R,4R)-1-(chrysen-6-yl)-3-hydroxy-4-(4-methoxyphenyl)azetidin-2-oneacetate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 0.5h;
DOI:10.1002/hlca.201100225

Reference yield: 85.0%

: 1215310-72-7
(3R,4R)-1-(chrysen-6-yl)-3-hydroxy-4-phenylazetidin-2-one

: 108-24-7
acetic anhydride

: 1215310-74-9,302595-58-0
(3R,4R)-1-(chrysen-6-yl)-3-hydroxy-4-(4-methoxyphenyl)azetidin-2-oneacetate

Guidance literature:: With triethylamine;

Reference yield:

: 1357362-60-7
(3R,4R)-3-{[(1S,3R,4R,6R)-4-bromo-3,7,7-trimethylbicyclo[4.1.0]hept-3-yl]oxy}-1-(chrysen-6-yl)-4-phenylazetidin-2-one

: 1215310-74-9,302595-58-0
(3R,4R)-1-(chrysen-6-yl)-3-hydroxy-4-(4-methoxyphenyl)azetidin-2-oneacetate

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; zinc / methanol / 80 °C

2: triethylamine / dichloromethane / 0.5 h / 0 - 20 °C

With acetic acid; triethylamine; zinc; In methanol; dichloromethane;
DOI:10.1002/hlca.201100225