C₃₁H₃₉N₃O₆Si

Base Information

Chemical Name:C₃₁H₃₉N₃O₆Si
CAS No.:938071-33-1
Molecular Formula:C₃₁H₃₉N₃O₆Si
Molecular Weight:577.753
Hs Code.:

C<sub>31</sub>H<sub>39</sub>N<sub>3</sub>O<sub>6</sub>Si

Synonyms:C₃₁H₃₉N₃O₆Si

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Chemical Property of C₃₁H₃₉N₃O₆Si

Chemical Property:

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Technology Process of C₃₁H₃₉N₃O₆Si

There total 11 articles about C₃₁H₃₉N₃O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 938071-26-2
(E)-methyl 2-[(3-tert-butyldimethylsilyloxy-4-methoxyphenyl)propenoylamino]-3-oxobutanoate

: 938071-33-1
C₃₁H₃₉N₃O₆Si

Guidance literature:: Multi-step reaction with 7 steps

1: 81 percent / triethylamine; triphenylphosphine; iodine / CH₂Cl₂ / 20 °C

2: 93 percent / DIBAL / CH₂Cl₂

3: 92 percent / Dess-Martin periodinane / CH₂Cl₂

4: 53 percent / zinc; 1,2-dibromoethane; trimethylsilyl chloride / boron-trifluoride-etherate / tetrahydrofuran / 3 h

5: 76 percent / Dess-Martin periodinane / CH₂Cl₂ / 0.33 h / 20 °C

6: barium hydroxide / tetrahydrofuran; H₂O

7: PyBOP; i-Pr₂NEt / CH₂Cl₂

With barium dihydroxide; chloro-trimethyl-silane; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; iodine; diisobutylaluminium hydride; Dess-Martin periodane; ethylene dibromide; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; zinc; boron-trifluoride-etherate; In tetrahydrofuran; dichloromethane; water;
DOI:10.1039/b618160k

Reference yield:

: 3-hydroxy-4-methoxycinnamamide

: 938071-33-1
C₃₁H₃₉N₃O₆Si

Guidance literature:: Multi-step reaction with 9 steps

1: 70 percent / imidazole / dimethylformamide

2: 90 percent / dirhodium tetraacetate / CH₂Cl₂ / 4 h / Heating

3: 81 percent / triethylamine; triphenylphosphine; iodine / CH₂Cl₂ / 20 °C

4: 93 percent / DIBAL / CH₂Cl₂

5: 92 percent / Dess-Martin periodinane / CH₂Cl₂

6: 53 percent / zinc; 1,2-dibromoethane; trimethylsilyl chloride / boron-trifluoride-etherate / tetrahydrofuran / 3 h

7: 76 percent / Dess-Martin periodinane / CH₂Cl₂ / 0.33 h / 20 °C

8: barium hydroxide / tetrahydrofuran; H₂O

9: PyBOP; i-Pr₂NEt / CH₂Cl₂

With 1H-imidazole; barium dihydroxide; chloro-trimethyl-silane; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; iodine; diisobutylaluminium hydride; Dess-Martin periodane; ethylene dibromide; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; zinc; dirhodium tetraacetate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/b618160k

Reference yield:

: 938071-31-9
[2-(3-tert-butyldimethylsiloxy-4-methoxystyryl)-5-methyloxazol-4-yl]methanol

: 938071-33-1
C₃₁H₃₉N₃O₆Si

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / Dess-Martin periodinane / CH₂Cl₂

2: 53 percent / zinc; 1,2-dibromoethane; trimethylsilyl chloride / boron-trifluoride-etherate / tetrahydrofuran / 3 h

3: 76 percent / Dess-Martin periodinane / CH₂Cl₂ / 0.33 h / 20 °C

4: barium hydroxide / tetrahydrofuran; H₂O

5: PyBOP; i-Pr₂NEt / CH₂Cl₂

With barium dihydroxide; chloro-trimethyl-silane; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; Dess-Martin periodane; ethylene dibromide; N-ethyl-N,N-diisopropylamine; zinc; boron-trifluoride-etherate; In tetrahydrofuran; dichloromethane; water;
DOI:10.1039/b618160k