N₂-(3-chloro-4-fluorophenyl)-6-(4-nitrophenoxy)-N₄-(4-nitrophenyl)-1,3,5-triazine-2,4-diamine

Base Information

• Chemical Name: N₂-(3-chloro-4-fluorophenyl)-6-(4-nitrophenoxy)-N₄-(4-nitrophenyl)-1,3,5-triazine-2,4-diamine
• CAS No.: 1360627-54-8
• Molecular Formula: C₂₁H₁₃ClFN₇O₅
• Molecular Weight: 497.83

Synonyms:N₂-(3-chloro-4-fluorophenyl)-6-(4-nitrophenoxy)-N₄-(4-nitrophenyl)-1,3,5-triazine-2,4-diamine

Chemical Property of N₂-(3-chloro-4-fluorophenyl)-6-(4-nitrophenoxy)-N₄-(4-nitrophenyl)-1,3,5-triazine-2,4-diamine

Chemical Property:

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Technology Process of N₂-(3-chloro-4-fluorophenyl)-6-(4-nitrophenoxy)-N₄-(4-nitrophenyl)-1,3,5-triazine-2,4-diamine

There total 3 articles about N₂-(3-chloro-4-fluorophenyl)-6-(4-nitrophenoxy)-N₄-(4-nitrophenyl)-1,3,5-triazine-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + C15H9Cl2FN6O2 → N2-(3-chloro-4-fluorophenyl)-6-(4-nitrophenoxy)-N4-(4-nitrophenyl)-1,3,5-triazine-2,4-diamine (1360627-54-8)

Guidance literature:

With sodium carbonate; In 1,4-dioxane; at 60 - 65 ℃;

DOI:10.2174/157018012799129936

Reference yield:

C9H4Cl3FN4 (1174140-78-3) → N2-(3-chloro-4-fluorophenyl)-6-(4-nitrophenoxy)-N4-(4-nitrophenyl)-1,3,5-triazine-2,4-diamine (1360627-54-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: acetone / 20 °C

1.2: 20 °C

2.1: sodium carbonate / 1,4-dioxane / 60 - 65 °C

With sodium carbonate; In 1,4-dioxane; acetone;

DOI:10.2174/157018012799129936

Reference yield:

3-chloro-4-fluorophenylamine (367-21-5) → N2-(3-chloro-4-fluorophenyl)-6-(4-nitrophenoxy)-N4-(4-nitrophenyl)-1,3,5-triazine-2,4-diamine (1360627-54-8)

Guidance literature:

Multi-step reaction with 3 steps

1.1: acetone / 2 h / 0 - 5 °C

2.1: acetone / 20 °C

2.2: 20 °C

3.1: sodium carbonate / 1,4-dioxane / 60 - 65 °C

With sodium carbonate; In 1,4-dioxane; acetone;

DOI:10.2174/157018012799129936

upstream raw materials:

4-nitro-phenol

C₉H₄Cl₃FN₄

3-chloro-4-fluorophenylamine

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