3-O-benzyl-N-benzyloxycarbonyladrenaline 4-O-<β-(triacetyl-glucuronide methylester)>

Base Information

Chemical Name:3-O-benzyl-N-benzyloxycarbonyladrenaline 4-O-<β-(triacetyl-glucuronide methylester)>
CAS No.:106148-98-5
Molecular Formula:C₃₇H₄₁NO₁₄
Molecular Weight:723.731
Hs Code.:

Synonyms:3-O-benzyl-N-benzyloxycarbonyladrenaline 4-O-<β-(triacetyl-glucuronide methylester)>

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Chemical Property of 3-O-benzyl-N-benzyloxycarbonyladrenaline 4-O-<β-(triacetyl-glucuronide methylester)>

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Technology Process of 3-O-benzyl-N-benzyloxycarbonyladrenaline 4-O-<β-(triacetyl-glucuronide methylester)>

There total 6 articles about 3-O-benzyl-N-benzyloxycarbonyladrenaline 4-O-<β-(triacetyl-glucuronide methylester)> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 106148-97-4
3-O-benzyl-N-benzyloxycarbonyladrenalone 4-O-<β-(triacetyl-glucuronide methylester)>

: 106148-98-5
3-O-benzyl-N-benzyloxycarbonyladrenaline 4-O-<β-(triacetyl-glucuronide methylester)>

Guidance literature:: With sodium tetrahydroborate; tetra(n-butyl)ammonium hydrogensulfate; In water; 1,2-dichloro-ethane; for 6h;

Reference yield:

: 101878-49-3
benzyl (2-(3,4-dihydroxyphenyl)-2-oxoethyl)(methyl)carbamate

: 106148-98-5
3-O-benzyl-N-benzyloxycarbonyladrenaline 4-O-<β-(triacetyl-glucuronide methylester)>

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / DMF, 1.) 0-5 deg C, 3 h, 2.) 24 h

2: 1.) NaOH / 1.) Bu₄NHSO₄ / 1.) H₂O/CH₂Cl₂, 10 min, 2.) CH₂Cl₂/Et₂O, overnight

3: 80 percent / NaBH₄ / Bu₄NHSO₄ / H₂O; 1,2-dichloro-ethane / 6 h

With sodium hydroxide; sodium tetrahydroborate; sodium hydride; tetra(n-butyl)ammonium hydrogensulfate; In water; 1,2-dichloro-ethane;

Reference yield:

: 62-13-5
1-(3,4-dihydroxyphenyl)-1-oxo-2-methylamino-ethan-hydrochlorid

: 106148-98-5
3-O-benzyl-N-benzyloxycarbonyladrenaline 4-O-<β-(triacetyl-glucuronide methylester)>

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / 2 N NaOH / toluene / 2 h / 5 - 10 °C

2: 1.) NaH / DMF, 1.) 0-5 deg C, 3 h, 2.) 24 h

3: 1.) NaOH / 1.) Bu₄NHSO₄ / 1.) H₂O/CH₂Cl₂, 10 min, 2.) CH₂Cl₂/Et₂O, overnight

4: 80 percent / NaBH₄ / Bu₄NHSO₄ / H₂O; 1,2-dichloro-ethane / 6 h

With sodium hydroxide; sodium tetrahydroborate; sodium hydride; tetra(n-butyl)ammonium hydrogensulfate; In water; 1,2-dichloro-ethane; toluene;