trans-4-Phenylbut-3-enylmethylether

Base Information

• Chemical Name: trans-4-Phenylbut-3-enylmethylether
• CAS No.: 20840-11-3
• Molecular Formula: C₁₁H₁₄O
• Molecular Weight: 162.232
• Mol file: 20840-11-3.mol

Synonyms:trans-4-Phenylbut-3-enylmethylether

Chemical Property of trans-4-Phenylbut-3-enylmethylether

Chemical Property:

Purity/Quality:

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Technology Process of trans-4-Phenylbut-3-enylmethylether

There total 1 articles about trans-4-Phenylbut-3-enylmethylether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethylene glycol dimethyl ether (111-96-6) + cyclopropyl phenyl ketone (3481-02-5) → trans-4-Phenylbut-3-enylmethylether (20840-11-3)

Guidance literature:

Multistep reaction; (i) B₂H₆, (ii) (heating), (iii) BF₃-Et₂O;

DOI:10.1016/S0040-4020(01)96826-7

Reference yield: 80.0%

trans-4-Phenylbut-3-enylmethylether (20840-11-3) + phenylselenyl triflate (112238-64-9) → (1RS,2SR)-1-azido-4-methoxy-1-phenyl-2-(phenylseleno)butane

Guidance literature:

With sodium azide; In acetonitrile; at 0 ℃; for 2h;

DOI:10.1080/00397919808007031

Reference yield:

trans-4-Phenylbut-3-enylmethylether (20840-11-3) → (1R,2R)-4-Methoxy-1-phenyl-butane-1,2-diol

Guidance literature:

With (3a,9R,3'''a,4'"b,9'"R)-9,9'-[1,4-phthalazinediylbis(oxy)]bis[6'-(methyloxy)-10,11-dihydrocinchonan]; osmium(VIII) oxide; methanesulfonamide; potassium carbonate; potassium hexacyanoferrate(III); In water; tert-butyl alcohol; at 0 ℃;

DOI:10.1016/S0040-4039(00)77153-X

upstream raw materials:

diethylene glycol dimethyl ether

cyclopropyl phenyl ketone