(R,R)-N,N’-bis-(1-benzyl-1,2,3-triazole-4-ylmethyl)-1,2-diphenylethylenediamine

Base Information

Chemical Name:(R,R)-N,N’-bis-(1-benzyl-1,2,3-triazole-4-ylmethyl)-1,2-diphenylethylenediamine
CAS No.:1402063-32-4
Molecular Formula:C₃₄H₃₄N₈
Molecular Weight:554.698
Hs Code.:

Synonyms:(R,R)-N,N’-bis-(1-benzyl-1,2,3-triazole-4-ylmethyl)-1,2-diphenylethylenediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R,R)-N,N’-bis-(1-benzyl-1,2,3-triazole-4-ylmethyl)-1,2-diphenylethylenediamine

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Technology Process of (R,R)-N,N’-bis-(1-benzyl-1,2,3-triazole-4-ylmethyl)-1,2-diphenylethylenediamine

There total 3 articles about (R,R)-N,N’-bis-(1-benzyl-1,2,3-triazole-4-ylmethyl)-1,2-diphenylethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1402063-31-3
(R,R)-N,N’-bis-propargyl-1,2-diphenylethylenediamine

: 622-79-7
benzyl azide

: 1402063-32-4
(R,R)-N,N’-bis-(1-benzyl-1,2,3-triazole-4-ylmethyl)-1,2-diphenylethylenediamine

Guidance literature:: With copper diacetate; sodium L-ascorbate; In water; tert-butyl alcohol; for 72h; Inert atmosphere;
DOI:10.1021/ol302354z DOI:10.1021/ol302354z

Reference yield:

: 100-39-0
benzyl bromide

: 1402063-32-4
(R,R)-N,N’-bis-(1-benzyl-1,2,3-triazole-4-ylmethyl)-1,2-diphenylethylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / dimethyl sulfoxide / 2 h / Inert atmosphere

2: copper diacetate; sodium L-ascorbate / tert-butyl alcohol; water / 72 h / Inert atmosphere

With sodium azide; copper diacetate; sodium L-ascorbate; In water; dimethyl sulfoxide; tert-butyl alcohol;
DOI:10.1021/ol302354z DOI:10.1021/ol302354z

Reference yield:

: 35132-20-8
(R,R)-1,2-diphenylethylenediamine

: 1402063-32-4
(R,R)-N,N’-bis-(1-benzyl-1,2,3-triazole-4-ylmethyl)-1,2-diphenylethylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile; toluene / 24 h / 80 °C / Inert atmosphere

2: copper diacetate; sodium L-ascorbate / tert-butyl alcohol; water / 72 h / Inert atmosphere

With copper diacetate; potassium carbonate; sodium L-ascorbate; In water; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ol302354z DOI:10.1021/ol302354z