cis-triphenylphosphane pyridine tetracarbonyltungsten

Base Information

Chemical Name:cis-triphenylphosphane pyridine tetracarbonyltungsten
CAS No.:38496-28-5
Molecular Formula:C₂₇H₂₀NO₄PW
Molecular Weight:637.284
Hs Code.:

Synonyms:cis-triphenylphosphane pyridine tetracarbonyltungsten

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Chemical Property of cis-triphenylphosphane pyridine tetracarbonyltungsten

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Technology Process of cis-triphenylphosphane pyridine tetracarbonyltungsten

There total 3 articles about cis-triphenylphosphane pyridine tetracarbonyltungsten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 110-86-1
pyridine

: 18078-18-7,476313-51-6
cis-{W(CO)4P(C₆H₅)3(acetonitrile)}

: 38496-28-5
cis-triphenylphosphane pyridine tetracarbonyltungsten

Guidance literature:: In benzene; at 80 ℃; Inert atmosphere;
DOI:10.1002/mrc.3925

Reference yield: 68.0%

: 16743-01-4,40903-14-8
cis-tetracarbonyldi(pyridine-N)tungsten⁽⁰⁾

: 38496-28-5
cis-triphenylphosphane pyridine tetracarbonyltungsten

Guidance literature:: With tetraethylammonium perchlorate; triphenylphosphine; In acetonitrile; Electrochem. Process; under Ar, set of Pt electrodes inserted into stirred MeCN soln. of W complex and PPh3 (1:1 molar ratio) (contg. 0.1 M Et4NClO4 as supporting electrolite), potential of 0.2 V vs. satd. NaCl SCE applied within 15 min at 22°C; pptn. with water; IR anal.;
DOI:10.1021/ja00375a016

Reference yield: 40.0%

: 16743-01-4,40903-14-8
tetracarbonylbis(pyridine)tungsten⁽⁰⁾

: 603-35-0
triphenylphosphine

: 16743-03-6,38800-77-0,68738-00-1
trans-triphenylphosphane tetracarbonyltungsten

: 38496-28-5
cis-triphenylphosphane pyridine tetracarbonyltungsten

Guidance literature:: In benzene; starting complex suspended in benzene, triphenylphosphane added, mixt. stirred for 24 h at 40-45 °C; solvent evapd., column chromy., elem. anal.;
DOI:10.1002/1099-0682(200109)2001:9<2255::AID-EJIC2255>3.0.CO;2-P