2-[3,5-bis[(4,6-dimethylpyridin-2-ylcarbamoyl)methyl]-2,4,6-trimethylphenyl]-N-(4,6-dimethylpyridin-2-yl)acetamide

Base Information

Chemical Name:2-[3,5-bis[(4,6-dimethylpyridin-2-ylcarbamoyl)methyl]-2,4,6-trimethylphenyl]-N-(4,6-dimethylpyridin-2-yl)acetamide
CAS No.:797818-03-2
Molecular Formula:C₃₆H₄₂N₆O₃
Molecular Weight:606.768
Hs Code.:

Synonyms:2-[3,5-bis[(4,6-dimethylpyridin-2-ylcarbamoyl)methyl]-2,4,6-trimethylphenyl]-N-(4,6-dimethylpyridin-2-yl)acetamide

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Chemical Property of 2-[3,5-bis[(4,6-dimethylpyridin-2-ylcarbamoyl)methyl]-2,4,6-trimethylphenyl]-N-(4,6-dimethylpyridin-2-yl)acetamide

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Technology Process of 2-[3,5-bis[(4,6-dimethylpyridin-2-ylcarbamoyl)methyl]-2,4,6-trimethylphenyl]-N-(4,6-dimethylpyridin-2-yl)acetamide

There total 3 articles about 2-[3,5-bis[(4,6-dimethylpyridin-2-ylcarbamoyl)methyl]-2,4,6-trimethylphenyl]-N-(4,6-dimethylpyridin-2-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 5407-87-4
2-Amino-4,6-dimethylpyridine

: 797818-06-5
(3,5-bis-chlorocarbonylmethyl-2,4,6-trimethyl-phenyl)-acetyl chloride

: 797818-03-2
2-[3,5-bis[(4,6-dimethylpyridin-2-ylcarbamoyl)methyl]-2,4,6-trimethylphenyl]-N-(4,6-dimethylpyridin-2-yl)acetamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1021/jo048979k

Reference yield:

: 2-{3,5-Bis-[(4,6-dimethyl-pyridin-2-ylcarbamoyl)-methyl]-2,4,6-trimethyl-phenyl}-N-(4,6-dimethyl-pyridin-2-yl)-acetamide; compound with (2R,3S,4S,5R,6R)-2-hydroxymethyl-6-octyloxy-tetrahydro-pyran-3,4,5-triol

: 29836-26-8
n-octyl β-D-glucopyranoside

: 797818-03-2
2-[3,5-bis[(4,6-dimethylpyridin-2-ylcarbamoyl)methyl]-2,4,6-trimethylphenyl]-N-(4,6-dimethylpyridin-2-yl)acetamide

Guidance literature:: In chloroform-d1; at 24.85 ℃; Equilibrium constant;
DOI:10.1021/jo048979k

Reference yield:

: 40207-09-8
(2,4,6-Trimethylbenzene)-1,3,5-triacetic acid

: 797818-03-2
2-[3,5-bis[(4,6-dimethylpyridin-2-ylcarbamoyl)methyl]-2,4,6-trimethylphenyl]-N-(4,6-dimethylpyridin-2-yl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂

2: 65 percent / triethylamine / CH₂Cl₂ / 24 h / 20 °C

With thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1021/jo048979k