3R-1-Chloro-2-oxo-3-N-(benzyloxycarbonyl)amino-4-(naphth-2-ylthio) butane

Base Information

Chemical Name:3R-1-Chloro-2-oxo-3-N-(benzyloxycarbonyl)amino-4-(naphth-2-ylthio) butane
CAS No.:159877-95-9
Molecular Formula:C₂₂H₂₀ClNO₃S
Molecular Weight:413.925
Hs Code.:

Synonyms:3R-1-Chloro-2-oxo-3-N-(benzyloxycarbonyl)amino-4-(naphth-2-ylthio) butane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3R-1-Chloro-2-oxo-3-N-(benzyloxycarbonyl)amino-4-(naphth-2-ylthio) butane

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Technology Process of 3R-1-Chloro-2-oxo-3-N-(benzyloxycarbonyl)amino-4-(naphth-2-ylthio) butane

There total 6 articles about 3R-1-Chloro-2-oxo-3-N-(benzyloxycarbonyl)amino-4-(naphth-2-ylthio) butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 159877-94-8
3R-1-Diazo-2-oxo-3-N-(benzyloxycarbonyl)amino-4-(naphth-2-ylthio) butane

: 159877-95-9
3R-1-Chloro-2-oxo-3-N-(benzyloxycarbonyl)amino-4-(naphth-2-ylthio) butane

Guidance literature:: With hydrogenchloride; In diethyl ether; at -20 ℃;
DOI:10.1021/jm9704098

Reference yield: 87.0%

: 159877-95-9
3R-1-Chloro-2-oxo-3-N-(benzyloxycarbonyl)amino-4-(naphth-2-ylthio) butane

Guidance literature:

Reference yield:

: 26054-60-4
((S)-2-Oxo-oxetan-3-yl)-carbamic acid benzyl ester

: 159877-95-9
3R-1-Chloro-2-oxo-3-N-(benzyloxycarbonyl)amino-4-(naphth-2-ylthio) butane

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) THF, RT, 15 min, 2.) THF, CH₂Cl₂, 1 h

2: Et₃N / ethyl acetate / -30 °C

3: ethyl acetate; diethyl ether / 0.33 h

4: 87 percent / HCl (g) / diethyl ether / -20 °C

With hydrogenchloride; sodium hydride; triethylamine; In diethyl ether; ethyl acetate;
DOI:10.1021/jm9704098