(R)-2-Benzyloxycarbonylamino-3-(naphthalen-2-ylsulfanyl)-propionic acid

Base Information

Chemical Name:(R)-2-Benzyloxycarbonylamino-3-(naphthalen-2-ylsulfanyl)-propionic acid
CAS No.:159877-93-7
Molecular Formula:C₂₁H₁₉NO₄S
Molecular Weight:381.452
Hs Code.:

Synonyms:(R)-2-Benzyloxycarbonylamino-3-(naphthalen-2-ylsulfanyl)-propionic acid

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Chemical Property of (R)-2-Benzyloxycarbonylamino-3-(naphthalen-2-ylsulfanyl)-propionic acid

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Technology Process of (R)-2-Benzyloxycarbonylamino-3-(naphthalen-2-ylsulfanyl)-propionic acid

There total 1 articles about (R)-2-Benzyloxycarbonylamino-3-(naphthalen-2-ylsulfanyl)-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26054-60-4
((S)-2-Oxo-oxetan-3-yl)-carbamic acid benzyl ester

: 91-60-1
2-Naphthalenethiol

: 159877-93-7
(R)-2-Benzyloxycarbonylamino-3-(naphthalen-2-ylsulfanyl)-propionic acid

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) THF, RT, 15 min, 2.) THF, CH₂Cl₂, 1 h;
DOI:10.1021/jm9704098

Reference yield:

: 159877-93-7
(R)-2-Benzyloxycarbonylamino-3-(naphthalen-2-ylsulfanyl)-propionic acid

: 543-27-1
isobutyl chloroformate

: C₂₆H₂₇NO₆S

Guidance literature:: With triethylamine; In ethyl acetate; at -30 ℃;
DOI:10.1021/jm9704098

Reference yield:

: 159877-93-7
(R)-2-Benzyloxycarbonylamino-3-(naphthalen-2-ylsulfanyl)-propionic acid

: [(R)-2-(Naphthalen-2-ylsulfanyl)-1-oxiranyl-ethyl]-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: Et₃N / ethyl acetate / -30 °C

2: ethyl acetate; diethyl ether / 0.33 h

3: 87 percent / HCl (g) / diethyl ether / -20 °C

4: 40 percent / NaBH₄ / tetrahydrofuran / 0.5 h

5: 99 percent / KOH / ethanol; ethyl acetate / 0.25 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; sodium tetrahydroborate; triethylamine; In tetrahydrofuran; diethyl ether; ethanol; ethyl acetate;
DOI:10.1021/jm9704098