N'-(4-ethoxymethoxy-benzyl)-hydrazinecarboxylic acid 9H-fluoren-9-ylmethyl ester

Base Information

Chemical Name:N'-(4-ethoxymethoxy-benzyl)-hydrazinecarboxylic acid 9H-fluoren-9-ylmethyl ester
CAS No.:808733-43-9
Molecular Formula:C₂₅H₂₆N₂O₄
Molecular Weight:418.492
Hs Code.:

<i>N</i>'-(4-ethoxymethoxy-benzyl)-hydrazinecarboxylic acid 9<i>H</i>-fluoren-9-ylmethyl ester

Synonyms:N'-(4-ethoxymethoxy-benzyl)-hydrazinecarboxylic acid 9H-fluoren-9-ylmethyl ester

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Chemical Property of N'-(4-ethoxymethoxy-benzyl)-hydrazinecarboxylic acid 9H-fluoren-9-ylmethyl ester

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Technology Process of N'-(4-ethoxymethoxy-benzyl)-hydrazinecarboxylic acid 9H-fluoren-9-ylmethyl ester

There total 3 articles about N'-(4-ethoxymethoxy-benzyl)-hydrazinecarboxylic acid 9H-fluoren-9-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 872554-73-9
N'-[1-(4-Ethoxymethoxy-phenyl)-meth-(E)-ylidene]-hydrazinecarboxylic acid 9H-fluoren-9-ylmethyl ester

: 808733-43-9
N'-(4-ethoxymethoxy-benzyl)-hydrazinecarboxylic acid 9H-fluoren-9-ylmethyl ester

Guidance literature:: With hydrogenchloride; sodium cyanoborohydride; In methanol; dichloromethane; for 0.5h;
DOI:10.1021/jo051585o

Reference yield:

: 35661-51-9
N-(9-fluorenylmethyloxycarbonyl)hydrazine

: 808733-43-9
N'-(4-ethoxymethoxy-benzyl)-hydrazinecarboxylic acid 9H-fluoren-9-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / CH₂Cl₂ / 24 h / 20 °C

2: 69 percent / sodium cyanoborohydride; hydrochloric acid / methanol; CH₂Cl₂ / 0.5 h

With hydrogenchloride; sodium cyanoborohydride; In methanol; dichloromethane;
DOI:10.1021/jo051585o

Reference yield:

: 128837-26-3
4-(ethyloxymethoxy)benzaldehyde

: 808733-43-9
N'-(4-ethoxymethoxy-benzyl)-hydrazinecarboxylic acid 9H-fluoren-9-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / CH₂Cl₂ / 24 h / 20 °C

2: 69 percent / sodium cyanoborohydride; hydrochloric acid / methanol; CH₂Cl₂ / 0.5 h

With hydrogenchloride; sodium cyanoborohydride; In methanol; dichloromethane;
DOI:10.1021/jo051585o