C₃₀H₄₉ClO₄Si

Base Information

Chemical Name:C₃₀H₄₉ClO₄Si
CAS No.:1032990-01-4
Molecular Formula:C₃₀H₄₉ClO₄Si
Molecular Weight:537.255
Hs Code.:

C<sub>30</sub>H<sub>49</sub>ClO<sub>4</sub>Si

Synonyms:C₃₀H₄₉ClO₄Si

Suppliers and Price of C₃₀H₄₉ClO₄Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₀H₄₉ClO₄Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₀H₄₉ClO₄Si

There total 12 articles about C₃₀H₄₉ClO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: C₃₀H₄₇ClO₄Si

: 1032990-01-4
C₃₀H₄₉ClO₄Si

Guidance literature:: With (triphenylphosphine)copper(I) hydride hexamer; phenylsilane; In toluene; at 0 - 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/c2ob25100k

Reference yield: 90.0%

: 1032989-88-0
C₃₀H₄₇ClO₄Si

: 1032990-01-4
C₃₀H₄₉ClO₄Si

Guidance literature:: With phenylsilane; [{(Ph₃P)CuH}]; In toluene;
DOI:10.1002/anie.200705565

Reference yield:

: 5470-84-8
4-benzyloxybutanal

: 1032990-01-4
C₃₀H₄₉ClO₄Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: piperidine / 5,5-dimethyl-1,3-cyclohexadiene / 0.5 h / 160 °C / Inert atmosphere

1.2: 3.5 h / 155 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere

3.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

4.1: dicyclohexylboron chloride; triethylamine / diethyl ether / 1 h / -78 - 0 °C / Inert atmosphere

4.2: 17 h / -78 - -20 °C / Inert atmosphere

5.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 - 20 °C

6.1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C / Inert atmosphere

6.2: 5 h / 0 - 20 °C / Inert atmosphere

7.1: sodium periodate / methanol / 0.5 h / 20 °C / pH 7 / aq. buffer; Inert atmosphere

8.1: dicyclohexylboron chloride; triethylamine / diethyl ether / 1 h / -78 - 0 °C / Inert atmosphere

8.2: 46 h / -78 - -20 °C / Inert atmosphere

9.1: methanesulfonyl chloride; triethylamine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

10.1: (triphenylphosphine)copper(I) hydride hexamer; phenylsilane / toluene / 0.5 h / 0 - 20 °C / Inert atmosphere

With piperidine; 2,6-dimethylpyridine; sodium tetrahydroborate; sodium periodate; lithium aluminium tetrahydride; (triphenylphosphine)copper(I) hydride hexamer; phenylsilane; dicyclohexylboron chloride; sodium hydrogencarbonate; Dess-Martin periodane; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; methanol; 5,5-dimethyl-1,3-cyclohexadiene; diethyl ether; dichloromethane; toluene; 1.1: Knoevenagel reaction / 1.2: Knoevenagel reaction / 3.1: Dess-Martin oxidation / 4.1: Aldol condensation / 4.2: Aldol condensation / 8.1: Aldol condensation / 8.2: Aldol condensation;
DOI:10.1039/c2ob25100k