(2?methylbenzyl)benzyl sulfide

Base Information

Chemical Name:(2?methylbenzyl)benzyl sulfide
CAS No.:222612-88-6
Molecular Formula:C₁₅H₁₆S
Molecular Weight:228.358
Hs Code.:

Synonyms:(2?methylbenzyl)benzyl sulfide

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Chemical Property of (2?methylbenzyl)benzyl sulfide

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Technology Process of (2?methylbenzyl)benzyl sulfide

There total 5 articles about (2?methylbenzyl)benzyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 100-39-0
benzyl bromide

: 552-45-4
1-chloromethyl-2-methylbenzene

: 222612-88-6
(2?methylbenzyl)benzyl sulfide

Guidance literature:: benzyl bromide; With thiourea; In methanol; Inert atmosphere; Reflux;

With sodium hydroxide; In methanol; Inert atmosphere; Reflux;

1-chloromethyl-2-methylbenzene; In methanol; at 20 ℃; Inert atmosphere; Reflux;
DOI:10.3998/ark.5550190.0011.921

Reference yield:

: 100-53-8
phenylmethanethiol

: 89-92-9
2-methylbenzyl bromide

: 222612-88-6
(2?methylbenzyl)benzyl sulfide

Guidance literature:: phenylmethanethiol; With potassium hydroxide; In methanol; at 70 ℃; for 0.25h; Inert atmosphere; Schlenk technique; Green chemistry;

2-methylbenzyl bromide; With copper(l) iodide; In methanol; at 110 ℃; for 12h; Inert atmosphere; Schlenk technique; Green chemistry;
DOI:10.1007/s10870-020-00859-w

Reference yield:

: 538-74-9
dibenzyl sulfide

: 222612-88-6
(2?methylbenzyl)benzyl sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / CH₂Cl₂ / 12 h / Ambient temperature

2: CsF / dimethylformamide / 12 h / Ambient temperature

With cesium fluoride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.47.267