Technology Process of zinc tetrakis-5,10,15-triphenyl-20-(4-(OCH2C(O)OCH3)-phenyl)-21H,23H-porphyrin
There total 1 articles about zinc tetrakis-5,10,15-triphenyl-20-(4-(OCH2C(O)OCH3)-phenyl)-21H,23H-porphyrin which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
condensation of the zinc-complex with methyl bromoacetate under mild basic conditions; purified by flash chromatography on Merck silica gel 60 (80-100 mesh) using CH2Cl2 as a solvent;
DOI:10.1021/jp0465175