meso‐5‐((4‐hydroxyphenyl)‐10,15,20‐tris(phenyl)porphyrinato)zinc(II)

Base Information

Chemical Name:meso‐5‐((4‐hydroxyphenyl)‐10,15,20‐tris(phenyl)porphyrinato)zinc(II)
CAS No.:110275-59-7
Molecular Formula:C₄₄H₂₈N₄OZn
Molecular Weight:694.123
Hs Code.:

Synonyms:meso‐5‐((4‐hydroxyphenyl)‐10,15,20‐tris(phenyl)porphyrinato)zinc(II)

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Chemical Property of meso‐5‐((4‐hydroxyphenyl)‐10,15,20‐tris(phenyl)porphyrinato)zinc(II)

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Technology Process of meso‐5‐((4‐hydroxyphenyl)‐10,15,20‐tris(phenyl)porphyrinato)zinc(II)

There total 6 articles about meso‐5‐((4‐hydroxyphenyl)‐10,15,20‐tris(phenyl)porphyrinato)zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 557-34-6
zinc diacetate

: 87345-22-0
5-(4'-hydroxyphenyl)-10,15,20-triphenylporphyrin

: 110275-59-7
meso‐5‐((4‐hydroxyphenyl)‐10,15,20‐tris(phenyl)porphyrinato)zinc(II)

Guidance literature:: In methanol; dichloromethane; Inert atmosphere;
DOI:10.1021/ja5052236

Reference yield: 90.0%

: 5970-45-6
zinc(II) acetate dihydrate

: 5-(4-hydroxyphenyl)-10,15,20-triphenylporphyrin

: 110275-59-7
meso‐5‐((4‐hydroxyphenyl)‐10,15,20‐tris(phenyl)porphyrinato)zinc(II)

Guidance literature:: In tetrahydrofuran; methanol; for 2h; Reflux; Inert atmosphere; Schlenk technique;
DOI:10.3390/molecules26123598

Reference yield: 3.56%

: 109-97-7,30604-81-0
pyrrole

: 557-34-6
zinc diacetate

: 100-52-7
benzaldehyde

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 110275-59-7
meso‐5‐((4‐hydroxyphenyl)‐10,15,20‐tris(phenyl)porphyrinato)zinc(II)

Guidance literature:: In propionic acid; distd. pyrrol mixed with soln. of C6H5COH and HOC6H4COH, refluxed for 4 h, solvent removed, CH3OH added, ppt. collected by filtration, washed (CH3OH-CHCl3), Zn(CH3COO)2 in CH3OH added, refluxed for 3 h; sovent evapd., residue extd. by CHCl3, org. layer concd., purified by chromy. (silica gel, CHCl3), second fraction collected, concd., purifn. repeated;
DOI:10.1021/jp0347419