dimethyltin(IV) diphthalanilate

Base Information

Chemical Name:dimethyltin(IV) diphthalanilate
CAS No.:155069-22-0
Molecular Formula:C₃₀H₂₆N₂O₆Sn
Molecular Weight:629.256
Hs Code.:

Synonyms:dimethyltin(IV) diphthalanilate

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Chemical Property of dimethyltin(IV) diphthalanilate

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Technology Process of dimethyltin(IV) diphthalanilate

There total 1 articles about dimethyltin(IV) diphthalanilate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 4727-29-1
phthalanilic acid

: 753-73-1
dimethyltin dichloride

: 155069-22-0
dimethyltin(IV) diphthalanilate

Guidance literature:: With sodium; In isopropyl alcohol; benzene; byproducts: NaCl; addn. of Na metal to an excess of isopropanol and benzene, addn. of phthalanilic acid in benzene under exclusion of moisture, refluxing for 1 h, cooling, addn. of Sn-compd. in benzene, refluxing for 4 h; filtn. to remove pptd. NaCl, removing solvent under reduced pressure, recrystn. from benzene/petroleum ether, elem. anal.;