Sulfuric acid mono-{(2R,3S,4S,5R)-3,4-dihydroxy-5-[(4-methoxy-benzyloxyimino)-methyl]-tetrahydro-furan-2-ylmethyl} ester

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Chemical Name:Sulfuric acid mono-{(2R,3S,4S,5R)-3,4-dihydroxy-5-[(4-methoxy-benzyloxyimino)-methyl]-tetrahydro-furan-2-ylmethyl} ester
CAS No.:365278-80-4
Molecular Formula:C₁₄H₁₉NO₉S
Molecular Weight:377.372
Hs Code.:

Synonyms:Sulfuric acid mono-{(2R,3S,4S,5R)-3,4-dihydroxy-5-[(4-methoxy-benzyloxyimino)-methyl]-tetrahydro-furan-2-ylmethyl} ester

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Chemical Property of Sulfuric acid mono-{(2R,3S,4S,5R)-3,4-dihydroxy-5-[(4-methoxy-benzyloxyimino)-methyl]-tetrahydro-furan-2-ylmethyl} ester

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Technology Process of Sulfuric acid mono-{(2R,3S,4S,5R)-3,4-dihydroxy-5-[(4-methoxy-benzyloxyimino)-methyl]-tetrahydro-furan-2-ylmethyl} ester

There total 3 articles about Sulfuric acid mono-{(2R,3S,4S,5R)-3,4-dihydroxy-5-[(4-methoxy-benzyloxyimino)-methyl]-tetrahydro-furan-2-ylmethyl} ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 46425-57-4
6-sulfo-2,5-anhydro-D-mannose

: O-(4-methoxybenzyl)-hydroxylamine HCl

: 365278-80-4
Sulfuric acid mono-{(2R,3S,4S,5R)-3,4-dihydroxy-5-[(4-methoxy-benzyloxyimino)-methyl]-tetrahydro-furan-2-ylmethyl} ester

Guidance literature:: In acetate buffer; at 20 ℃; for 0.333333h; pH=4;
DOI:10.1016/S0008-6215(01)00115-X

Reference yield:

: 2014-61-1
N-(4-methoxybenzyloxy)phthalimide

: 365278-80-4
Sulfuric acid mono-{(2R,3S,4S,5R)-3,4-dihydroxy-5-[(4-methoxy-benzyloxyimino)-methyl]-tetrahydro-furan-2-ylmethyl} ester

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / hydrazine hydrate; HCl / methanol / 3 h / 20 °C

2: 100 percent / acetate buffer / 0.33 h / 20 °C / pH 4

With hydrogenchloride; hydrazine hydrate; In methanol; acetate buffer;
DOI:10.1016/S0008-6215(01)00115-X

Reference yield:

: 105-13-5
4-Methoxybenzyl alcohol

: 365278-80-4
Sulfuric acid mono-{(2R,3S,4S,5R)-3,4-dihydroxy-5-[(4-methoxy-benzyloxyimino)-methyl]-tetrahydro-furan-2-ylmethyl} ester

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / PPh₃; DEAD / tetrahydrofuran / 20 °C

2: 64 percent / hydrazine hydrate; HCl / methanol / 3 h / 20 °C

3: 100 percent / acetate buffer / 0.33 h / 20 °C / pH 4

With hydrogenchloride; hydrazine hydrate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; acetate buffer;
DOI:10.1016/S0008-6215(01)00115-X