C₅₃H₉₇NO₁₂Si₂

Base Information

Chemical Name:C₅₃H₉₇NO₁₂Si₂
CAS No.:136391-42-9
Molecular Formula:C₅₃H₉₇NO₁₂Si₂
Molecular Weight:996.524
Hs Code.:

C<sub>53</sub>H<sub>97</sub>NO<sub>12</sub>Si<sub>2</sub>

Synonyms:C₅₃H₉₇NO₁₂Si₂

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Chemical Property of C₅₃H₉₇NO₁₂Si₂

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Technology Process of C₅₃H₉₇NO₁₂Si₂

There total 20 articles about C₅₃H₉₇NO₁₂Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.5%

: 136358-41-3,136457-97-1
C₆₁H₁₀₃NO₁₃Si₂

: 136391-42-9
C₅₃H₉₇NO₁₂Si₂

Guidance literature:: With 1,2-propanedithiol; diethylaluminium chloride; In dichloromethane; for 4h; Ambient temperature;

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 136391-42-9
C₅₃H₉₇NO₁₂Si₂

Guidance literature:: Multi-step reaction with 11 steps

1: 93 percent / 2,6-lutidine / CH₂Cl₂ / 0.25 h / -78 - 20 °C

2: 60.4 percent / dihydroquinidine acetate, OsO₄ / toluene / 5 h

3: 96 percent / H₂ / 10percent Pd(OH)2/C / ethyl acetate / 2 h

4: 80 percent / 4A molecular sieves, camphorsulfonic acid / benzene; tetrahydrofuran / 2 h / Ambient temperature

5: 95 percent / dicyclohexylcarbodiimide (DCC) / CH₂Cl₂ / 0.33 h

6: 90.8 percent / aq. LiOH / tetrahydrofuran; methanol / 2 h / -15 - -10 °C

7: N-metylmorpholine, (benzotriazolyl-1-oxy)tris(dimethylamino)phosphonium hexafluorophosphate (BOP) / CH₂Cl₂ / 3 h / Ambient temperature

8: 10percent aq. HCl / tetrahydrofuran / 0.08 h

9: Dess-Martin periodinane / CH₂Cl₂ / 1.5 h

10: LiCl, diazobicycloundecene (DBU) / acetonitrile / 2.5 h

11: 67.5 percent / Et₂AlCl, propanedithiol / CH₂Cl₂ / 4 h / Ambient temperature

With 4-methyl-morpholine; 2,6-dimethylpyridine; hydrogenchloride; lithium hydroxide; osmium(VIII) oxide; hydroquinidine acetate; 1,2-propanedithiol; 4 A molecular sieve; camphor-10-sulfonic acid; hydrogen; diethylaluminium chloride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; Dess-Martin periodane; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; lithium chloride; palladium dihydroxide; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; toluene; acetonitrile; benzene;

Reference yield:

: 136358-53-7,136358-54-8
<2R,S,3R,5S,6S,6(1S,2S)>-2-hydroxy-6-<2-(benzyloxy)-1-methoxy-3-methylbutyl>-5-methoxy-3-methyltetrahydropyran

: 136391-42-9
C₅₃H₉₇NO₁₂Si₂

Guidance literature:: Multi-step reaction with 12 steps

1: 73.5 percent / acetonitrile / 72 h / Heating

2: 93 percent / 2,6-lutidine / CH₂Cl₂ / 0.25 h / -78 - 20 °C

3: 60.4 percent / dihydroquinidine acetate, OsO₄ / toluene / 5 h

4: 96 percent / H₂ / 10percent Pd(OH)2/C / ethyl acetate / 2 h

5: 80 percent / 4A molecular sieves, camphorsulfonic acid / benzene; tetrahydrofuran / 2 h / Ambient temperature

6: 95 percent / dicyclohexylcarbodiimide (DCC) / CH₂Cl₂ / 0.33 h

7: 90.8 percent / aq. LiOH / tetrahydrofuran; methanol / 2 h / -15 - -10 °C

8: N-metylmorpholine, (benzotriazolyl-1-oxy)tris(dimethylamino)phosphonium hexafluorophosphate (BOP) / CH₂Cl₂ / 3 h / Ambient temperature

9: 10percent aq. HCl / tetrahydrofuran / 0.08 h

10: Dess-Martin periodinane / CH₂Cl₂ / 1.5 h

11: LiCl, diazobicycloundecene (DBU) / acetonitrile / 2.5 h

12: 67.5 percent / Et₂AlCl, propanedithiol / CH₂Cl₂ / 4 h / Ambient temperature

With 4-methyl-morpholine; 2,6-dimethylpyridine; hydrogenchloride; lithium hydroxide; osmium(VIII) oxide; hydroquinidine acetate; 1,2-propanedithiol; 4 A molecular sieve; camphor-10-sulfonic acid; hydrogen; diethylaluminium chloride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; Dess-Martin periodane; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; lithium chloride; palladium dihydroxide; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; toluene; acetonitrile; benzene;