1,1-dimethylethyl (4,4-dimethylcyclohexyl)(2-{[3′-(1,2,4-oxadiazol-3-yl)-4-biphenylyl]oxy}ethyl)carbamate

Base Information

Chemical Name:1,1-dimethylethyl (4,4-dimethylcyclohexyl)(2-{[3′-(1,2,4-oxadiazol-3-yl)-4-biphenylyl]oxy}ethyl)carbamate
CAS No.:1007579-37-4
Molecular Formula:C₂₉H₃₇N₃O₄
Molecular Weight:491.63
Hs Code.:

Synonyms:1,1-dimethylethyl (4,4-dimethylcyclohexyl)(2-{[3′-(1,2,4-oxadiazol-3-yl)-4-biphenylyl]oxy}ethyl)carbamate

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Chemical Property of 1,1-dimethylethyl (4,4-dimethylcyclohexyl)(2-{[3′-(1,2,4-oxadiazol-3-yl)-4-biphenylyl]oxy}ethyl)carbamate

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Technology Process of 1,1-dimethylethyl (4,4-dimethylcyclohexyl)(2-{[3′-(1,2,4-oxadiazol-3-yl)-4-biphenylyl]oxy}ethyl)carbamate

There total 9 articles about 1,1-dimethylethyl (4,4-dimethylcyclohexyl)(2-{[3′-(1,2,4-oxadiazol-3-yl)-4-biphenylyl]oxy}ethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1007579-36-3
1,1-dimethylethyl {2-[(3′-cyano-4-biphenylyl)oxy]ethyl}(4,4-dimethylcyclohexyl)carbamate

: 149-73-5
trimethyl orthoformate

: 1007579-37-4
1,1-dimethylethyl (4,4-dimethylcyclohexyl)(2-{[3′-(1,2,4-oxadiazol-3-yl)-4-biphenylyl]oxy}ethyl)carbamate

Guidance literature:: 1,1-dimethylethyl {2-[(3′-cyano-4-biphenylyl)oxy]ethyl}(4,4-dimethylcyclohexyl)carbamate; With hydroxylamine; In ethanol; at 20 ℃; for 70h;

trimethyl orthoformate; With toluene-4-sulfonic acid; In ethanol; water; at 100 ℃; for 1h; Sealed tube;

Reference yield:

: 1007579-36-3
1,1-dimethylethyl {2-[(3′-cyano-4-biphenylyl)oxy]ethyl}(4,4-dimethylcyclohexyl)carbamate

: 1007579-37-4
1,1-dimethylethyl (4,4-dimethylcyclohexyl)(2-{[3′-(1,2,4-oxadiazol-3-yl)-4-biphenylyl]oxy}ethyl)carbamate

Guidance literature:: With hydroxylamine; In ethanol; trimethyl orthoformate;

Reference yield:

: 26583-55-1
{2-[(4-bromophenyl)oxy]ethyl}amine

: 1007579-37-4
1,1-dimethylethyl (4,4-dimethylcyclohexyl)(2-{[3′-(1,2,4-oxadiazol-3-yl)-4-biphenylyl]oxy}ethyl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid; sodium cyanoborohydride / methanol / 20 °C

2.1: triethylamine / dichloromethane / 13 h

3.1: sodium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,2-dimethoxyethane / 5 h / 80 °C / Inert atmosphere

4.1: hydroxylamine / ethanol / 70 h / 20 °C

4.2: 1 h / 100 °C / Sealed tube

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; hydroxylamine; sodium cyanoborohydride; sodium carbonate; acetic acid; triethylamine; In methanol; 1,2-dimethoxyethane; ethanol; dichloromethane;