ethyl (4Z,6E)-9,9-bis[(benzylohy)methyl]-11methyldodeca-4,6,11-trienoate

Base Information

Chemical Name:ethyl (4Z,6E)-9,9-bis[(benzylohy)methyl]-11methyldodeca-4,6,11-trienoate
CAS No.:952688-01-6
Molecular Formula:C₃₁H₄₀O₄
Molecular Weight:476.656
Hs Code.:

Synonyms:ethyl (4Z,6E)-9,9-bis[(benzylohy)methyl]-11methyldodeca-4,6,11-trienoate

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Chemical Property of ethyl (4Z,6E)-9,9-bis[(benzylohy)methyl]-11methyldodeca-4,6,11-trienoate

Chemical Property:

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Technology Process of ethyl (4Z,6E)-9,9-bis[(benzylohy)methyl]-11methyldodeca-4,6,11-trienoate

There total 6 articles about ethyl (4Z,6E)-9,9-bis[(benzylohy)methyl]-11methyldodeca-4,6,11-trienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 952687-98-8
2-(2-methylallyl)-2-[(2E)-4-(tetrahydropyran-2-yloxy)but-2-enyl]propane-1,3-diol

: 952688-01-6
ethyl (4Z,6E)-9,9-bis[(benzylohy)methyl]-11methyldodeca-4,6,11-trienoate

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / NaH / dimethylformamide / 9 h / 20 °C

2: 95 percent / TsOH / methanol / 1.5 h / 20 °C

3: MnO₂ / CH₂Cl₂

4: 1.13 g / t-BuOK / tetrahydrofuran

With manganese(IV) oxide; potassium tert-butylate; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-2007-983774

Reference yield:

: 952687-99-9
2-{(E)-5,5-bis[(benzyloxy)methyl]-7-methylocta-2,7-dienyloxy}tetrahydro-2H-pyran

: 952688-01-6
ethyl (4Z,6E)-9,9-bis[(benzylohy)methyl]-11methyldodeca-4,6,11-trienoate

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / TsOH / methanol / 1.5 h / 20 °C

2: MnO₂ / CH₂Cl₂

3: 1.13 g / t-BuOK / tetrahydrofuran

With manganese(IV) oxide; potassium tert-butylate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1055/s-2007-983774

Reference yield:

: 952688-00-5
(E)-5,5-bis[(benzyloxy)methyl]7-methylocta-2,7-dien-1-ol

: 952688-01-6
ethyl (4Z,6E)-9,9-bis[(benzylohy)methyl]-11methyldodeca-4,6,11-trienoate

Guidance literature:: Multi-step reaction with 2 steps

1: MnO₂ / CH₂Cl₂

2: 1.13 g / t-BuOK / tetrahydrofuran

With manganese(IV) oxide; potassium tert-butylate; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-2007-983774