2-(9-(Benzolsulfonyl)-13-<(benzolsulfonyl)amino>-5,9-diazatridecyl)-2-nitrocyclododecanon

Base Information

Chemical Name:2-(9-(Benzolsulfonyl)-13-<(benzolsulfonyl)amino>-5,9-diazatridecyl)-2-nitrocyclododecanon
CAS No.:122866-38-0
Molecular Formula:C₃₅H₅₄N₄O₇S₂
Molecular Weight:706.968
Hs Code.:

Synonyms:2-(9-(Benzolsulfonyl)-13-<(benzolsulfonyl)amino>-5,9-diazatridecyl)-2-nitrocyclododecanon

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Chemical Property of 2-(9-(Benzolsulfonyl)-13-<(benzolsulfonyl)amino>-5,9-diazatridecyl)-2-nitrocyclododecanon

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Technology Process of 2-(9-(Benzolsulfonyl)-13-<(benzolsulfonyl)amino>-5,9-diazatridecyl)-2-nitrocyclododecanon

There total 4 articles about 2-(9-(Benzolsulfonyl)-13-<(benzolsulfonyl)amino>-5,9-diazatridecyl)-2-nitrocyclododecanon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 120269-91-2
4-(1-Nitro-2-oxocyclododec-1-yl)butanal

: 122890-17-9
4-(Benzolsulfonyl)-8-<(benzolsulfonyl)amino>-4-azaoctylamin

: 122866-38-0
2-(9-(Benzolsulfonyl)-13-<(benzolsulfonyl)amino>-5,9-diazatridecyl)-2-nitrocyclododecanon

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 9 ℃;
DOI:10.1002/hlca.19880710718

Reference yield:

: 4748-73-6
N-(cyanoethyl)-1,4-diaminobutane

: 122866-38-0
2-(9-(Benzolsulfonyl)-13-<(benzolsulfonyl)amino>-5,9-diazatridecyl)-2-nitrocyclododecanon

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / K₂CO₃ / 1.5 h / 60 °C

2: 1) H₂ / 1) PtO₂ / 1) EtOH, aq. HCl, 1 h, 23 deg C,3 atm; 2) EtOH, aq. HCl, 16 h, 3 atm

3: 66 percent / NaBH₄ / ethanol / 9 °C

With sodium tetrahydroborate; hydrogen; potassium carbonate; platinum(IV) oxide; In ethanol;
DOI:10.1002/hlca.19880710718

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 122866-38-0
2-(9-(Benzolsulfonyl)-13-<(benzolsulfonyl)amino>-5,9-diazatridecyl)-2-nitrocyclododecanon

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / K₂CO₃ / 1.5 h / 60 °C

2: 1) H₂ / 1) PtO₂ / 1) EtOH, aq. HCl, 1 h, 23 deg C,3 atm; 2) EtOH, aq. HCl, 16 h, 3 atm

3: 66 percent / NaBH₄ / ethanol / 9 °C

With sodium tetrahydroborate; hydrogen; potassium carbonate; platinum(IV) oxide; In ethanol;
DOI:10.1002/hlca.19880710718